| 茵陈五苓糖浆质量标准研究 |
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| 引用本文： | 章为,丁野,李文莉,李晓燕,李文波.茵陈五苓糖浆质量标准研究[J].中国药师,2012,15(1):33-35. |
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| 作者姓名： | 章为 丁野 李文莉 李晓燕 李文波 |
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| 作者单位： | 1. 湖南省食品药品检验研究院 长沙410001
2. 长沙市中心医院 |
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| 基金项目： | 国家药品标准提高行动计划(编号:67) |
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| 摘 要： | 目的:完善茵陈五苓糖浆的质量标准.方法:采用TLC法鉴别方中桂枝、茵陈；采用HPLC法测定方中绿原酸含量.结果:薄层鉴别特征明显,专属性强.HPLC法测定绿原酸在0.033 ～0.602 μg范围内有良好的线性关系,r=0.999 8,平均回收率为99.8％,RSD=1.4％(n=6).结论:本方法简便、可靠、准确,可用于茵陈五苓糖浆的质量控制.
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| 关 键 词： | 茵陈五苓糖浆 薄层色谱法 高效液相色谱法 质量标准 |
| 收稿时间： | 9/9/2011 12:00:00 AM |
| 修稿时间： | 2011/10/28 0:00:00 |
Study on Quality Standard for Yinchen Wuling Syrups |
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| Zhang Wei,Ding Ye,Li Wenli,Li Xiaoyan and Li Wenbo.Study on Quality Standard for Yinchen Wuling Syrups[J].China Pharmacist,2012,15(1):33-35. |
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| Authors: | Zhang Wei Ding Ye Li Wenli Li Xiaoyan and Li Wenbo |
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| Institution: | unan Institute for Food and Drug Control,Changsha 410001,China;unan Institute for Food and Drug Control,Changsha 410001,China;unan Institute for Food and Drug Control,Changsha 410001,China;unan Institute for Food and Drug Control,Changsha 410001,China;Changsha Central Hospital |
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| Abstract: | Objective： To improve the quality standard for Yinchen Wuling syrups. Method： Ramulus Cinnamomi and Herba Arte- misiae scopariae were indentified by TLC. The content of chlorogenic acid was determined by HPLC. Result： The characteristics of i- dentification by TLC were distinct and highly specific. The linear range of chlorogenic acid was 0. 033-0. 602 p,g, r = 0. 999 8. The aver- age recovery was 99.8% with RSD of 1.4% （n = 6）. Conclusion： The developed method is simple, accurate and suitable for the quali- ty control of Yinchen Wuling syrups. |
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| Keywords: | Yinchen Wuling syrups TLC HPLC Quality standard |
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