| 紫茵糖浆中丹参素的含量测定 |
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| 引用本文： | 周荣丽,丁菊英,丰连功,梁民琦,尹向明.紫茵糖浆中丹参素的含量测定[J].中国药业,2007,16(3):25-26. |
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| 作者姓名： | 周荣丽 丁菊英 丰连功 梁民琦 尹向明 |
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| 作者单位： | 胜利油田中心医院,山东,东营,257034 |
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| 摘 要： | 目的建立紫菌糖浆中丹参素含量的测定方法。方法采用高效液相色谱法，色谱柱为Hypersil ODS C18（250mm×4．6mm，5μm）；流动相为甲醇-0.5％醋酸（1：8），检测波长为281nm，流速为1．0mL／min。结果丹参素的回收率为99．67％，RSD为0．51％（n=6）。结论高效液相色谱法简便、快速、准确，可作为紫菌糖浆的质量控制方法。
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| 关 键 词： | 丹参素 高效液相色谱法 紫菌糖浆 |
| 文章编号： | 1006-4931（2007）03-0025-02 |
| 收稿时间： | 2006-05-15 |
| 修稿时间： | 2006-08-28 |
Determination of Danshensu in Ziyin Syrup |
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| Zhou Rongli,Ding Juying,Feng Liangong,Liang Minqi,Yin Xiangming.Determination of Danshensu in Ziyin Syrup[J].China Pharmaceuticals,2007,16(3):25-26. |
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| Authors: | Zhou Rongli Ding Juying Feng Liangong Liang Minqi Yin Xiangming |
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| Institution: | Zhou Rongli, Ding Juying, Feng Lian＇ gong, Liang Minqi, Yin Xiangming , (Shengli Oilfield Central Hospital, Dongying, Shandong, China 257034) |
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| Abstract: | Objective To establish an assay method for Danshensu in Ziyin syrup. Methods HPLC method was used. The chromatographic column was Hypersil ODS C18 （250 min×4.6 mm, 5 μm）.The mobile phase consisted of methanol-0.5% acetic acid （1：8）. Detective wavelength was at 281 nm. The flow rate was 1.0 mL/min. Results The average recover rate of Danshensu and relative standard deviation were 99. 67% and 0, 51% （n = 6）, respectively. Conclusion The method is simple, rapid and accurate. It may be used for the quality control of Ziyin syrup. |
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| Keywords: | Danshensu HPLC Ziyin syrup |
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