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| 毛细管气相色谱法测定栽培黄芩中有机氯农药残留量 | |
| 引用本文： | 王秀敏,邓英杰,张修宇,范玉玲,赵春杰,王栋.毛细管气相色谱法测定栽培黄芩中有机氯农药残留量[J].沈阳药科大学学报,2006,23(3):156-158. |
| 作者姓名： | 王秀敏 邓英杰 张修宇 范玉玲 赵春杰 王栋 |
| 作者单位： | 1. 沈阳药科大学,药学院,辽宁,沈阳110016 2. 哈尔滨商业大学,药物所博士后科研工作站,黑龙江,哈尔滨,150076 3. 黑龙江中医药大学,药学院,黑龙江,哈尔滨150040 |
| 摘 要： | 目的建立测定栽培黄芩中有机氯农药六六六、滴滴涕9个组分残留量的方法。方法采用在线提取,硫酸磺化后直接测定法;选用DB-1毛细管柱,通过柱程序升温手段,对9种农药进行分离测定。结果所测定的3批栽培黄芩样品和1批野生黄芩中总六六六和总滴滴涕的质量分数均小于等于1.463×10-5%。结论可用于栽培黄芩的有机氯农药测定。所测定样品及野生对照药材有机氯农药残留量均低于相关标准,可以安全使用。 |
| 关 键 词： | 毛细管气相色谱 黄芩 有机氯农药残留 |
| 文章编号： | 1006-2858(2006)03-0156-03 |
| 收稿时间： | 2004-11-08 |
| 修稿时间： | 2004年11月8日 |
Determination of organochlorine pesticide residues in Scutellaria baicalensis Georgi by GC-ECD |
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| WANG Xiu-min,DENG Ying-jie,ZHANG Xiu-yu,FAN Yu-ling,ZHAO Chun-jie,WANG Dong.Determination of organochlorine pesticide residues in Scutellaria baicalensis Georgi by GC-ECD[J].Journal of Shenyang Pharmaceutical University,2006,23(3):156-158. | |
| Authors: | WANG Xiu-min DENG Ying-jie ZHANG Xiu-yu FAN Yu-ling ZHAO Chun-jie WANG Dong |
| Abstract: | Objective To determine the residues of benzenehexachloride(BHC) and dichlorodiphenyl dichloro-ethylene(DDT) in Scutellaria baicalensis Georgi.Methods The organic chloride pesticide(OCPs) in the samples were extracted with acetone on line and separated by DB-1 capillary column with programmed temperature gas chromatography,all the 9 ingredients were seperated absolutely.Results Total amount of OCPs in these 10 samples were lower than 146.3 ng·g~(-1).Conclusions This method is rapid,simple and accurate.The OCPs of the two samples and the wilding Scutellaria are lower than the corresponding standards. |
| Keywords: | GC-ECD Scutellaria baicalensis Georgi organic chloride pesticides residue |
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