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头花蓼的化学成分
引用本文:于 明,李占林,李 宁,李 铣.头花蓼的化学成分[J].沈阳药科大学学报,2008,25(8):633-635.
作者姓名:于 明  李占林  李 宁  李 铣
作者单位:[1]辽宁省食品药品检验所,辽宁沈阳110023 [2]沈阳药科大学中药学院,辽宁沈阳110016
摘    要:目的对头花蓼(Polygonum capitatum Buch-Ham ex D.Don)体积分数为70%的乙醇溶液提取物的化学成分进行研究。方法利用各种色谱技术进行分离纯化,根据理化性质和波谱数据进行结构鉴定。结果得到11个化合物,分别鉴定为:槲皮素(1)、山柰酚(2)、槲皮苷(3)、原儿茶酸(4)、没食子酸(5)、原儿茶酸乙酯(6)、没食子酸乙酯(7)、香草酸(8)、1,5,7-三羟基-3-甲基蒽醌(9)、琥珀酸(10)、5-羟甲基糠醛(11)。结论化合物6、7、9、11为首次从该属植物中分离得到。

关 键 词:头花蓼  化学成分  结构鉴定
收稿时间:2007-9-25

Chemical constituents of the aerial parts of Polygonum capitatum
YU Ming,LI Zhan-lin,LI Ning,LI Xian.Chemical constituents of the aerial parts of Polygonum capitatum[J].Journal of Shenyang Pharmaceutical University,2008,25(8):633-635.
Authors:YU Ming  LI Zhan-lin  LI Ning  LI Xian
Institution:1.Liaoning Province Institute of Food and Drug Control, shenyang 110023,China; 2.School of Traditional Chinese Materia Medica, Shenyang Pharmaceutical University, Shenyang, 110016, China
Abstract:Objective To study the chemical constituents of the 70% ethanol extract of the aerial parts of Polygonum capitatum Buch-Ham ex D. Don. Methods The constituents were isolated by several chromatography methods and identified by physico-chemical characters and spectroscopic analysis. Results Eleven compounds were isolated and identified as: quercetin (1) , kaempferol (2), quercitrin (3) , protocatechuic acid (4), gallic acid (5) , protocatechuic acid ethyl ester (6) ,ethyl gallate (7), vanillic acid (8) , 1,5,7-trihydroxyl-3-methylanthraquinone (9), succinic acid (10) , 5-hydroxymethylfuraldehyde (11).Conclusion Compounds 6,7,9,11 are isolated from this genus for the first time.
Keywords:Polygonum capitatum Buch-Ham ex D  Polygonum capitatum Buch-Ham ex D" target="_blank">Don')">Polygonum capitatum Buch-Ham ex D  Don  chemical constituent  structural determination
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