| 壮骨健膝颗粒的质量标准研究 |
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| 引用本文： | 池志珍,黄巧文,郑芳.壮骨健膝颗粒的质量标准研究[J].海峡药学,2011,23(10):44-46. |
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| 作者姓名： | 池志珍 黄巧文 郑芳 |
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| 作者单位： | 福建中医药大学附属人民医院 福州350004 |
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| 摘 要： | 目的提高壮骨健膝颗粒的质量标准。方法用薄层色谱法鉴别颗粒中的川牛膝、徐长卿；用高效液相色谱法测定丹皮酚含量。结果在薄层色谱中可以检出川牛膝、徐长卿；丹皮酚在1．12-16．8μg·mL-1（r=0．9999）范围内线性关系良好，平均加样回收率为98．40％，RSD为1．16％（n=6）。结论方法简便，准确，专属性强，可以更有效地控制壮骨健膝颗粒的质量。
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| 关 键 词： | 川牛膝 徐长卿 薄层色谱法 丹皮酚 |
The study of quality standards of Zhuanggujianxi granules |
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| CHI Zhi-zhen,HUANG Qiao-wen,ZHENG Fang.The study of quality standards of Zhuanggujianxi granules[J].Strait Pharmaceutical Journal,2011,23(10):44-46. |
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| Authors: | CHI Zhi-zhen HUANG Qiao-wen ZHENG Fang |
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| Institution: | CHI Zhi-zhen,HUANG Qiao-wen,ZHENG Fang(The people's hospital affiliated to FUTCM,Fuzhou,350004,China) |
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| Abstract: | OBJECTIVE To improve the quality standards of Zhuanggujianxi Granule.METHODS TLC was employed to identify Cyathula officinalis Kuan and Cynanchum paniculatum(Bge.)Kitag in granule;high performance liquid chromatography was used to determine paeonol content in Zhuanggujianxi Granule.RESULTS Cyathula officinalis Kuan and Cynanchum paniculatum(Bge.)Kitag can be detected by TLC;The linearity was obtained over the range of 1.12~16.8μg·mL-1(r=0.9999)for paeonol,The average recoveries of was 98.40%,and the RSDs was 1.16%(n=6).CONCLUSION The method is simple,accurate,specific,and can more effectively control the quality of Zhuanggujianxi Granule. |
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| Keywords: | Paeonol HPLC TLC Zhuanggujianxi granule |
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