| 市售西红花药材掺伪染色检测方法的实验研究 |
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| 引用本文： | 付凌燕,闵春艳,汪祺,鲁静.市售西红花药材掺伪染色检测方法的实验研究[J].药物分析杂志,2012(1):74-77. |
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| 作者姓名： | 付凌燕 闵春艳 汪祺 鲁静 |
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| 作者单位： | 吉林省吉林市药品检验所;江苏省苏州市药品检验所;中国食品药品检定研究院 |
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| 基金项目： | 中药中有害残留物检测技术标准平台项目(2009ZX09308-006) |
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| 摘 要： | 目的:确认西红花药材中违法染色的色素或染料成分,建立相应的染色成分分析方法。方法:采用液相色谱-质谱联用以及对照试剂对照的方法,对染色成分进行鉴定;薄层色谱和高效液相色谱法检测染色物成分。结果:西红花药材掺伪染色的主要成分为柠檬黄、胭脂红、金胺O和新品红;对43批市售西红花药材进行了检测,其中32批检测出含有上述4种染色物,存在染色情况。结论:建立的检测方法可快速进行西红花药材中掺伪染色的定性检测。
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| 关 键 词： | 西红花 掺伪 薄层色谱法 高效液相色谱法 液-质联用分析 柠檬黄 胭脂红 金胺O 新品红 中药染色监测 |
Experimental research on the detection methods of Croci Stigma adulteration on the markets |
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| FU Ling-yan,MIN Chun-yan,WANG Qi,LU Jing.Experimental research on the detection methods of Croci Stigma adulteration on the markets[J].Chinese Journal of Pharmaceutical Analysis,2012(1):74-77. |
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| Authors: | FU Ling-yan MIN Chun-yan WANG Qi LU Jing |
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| Institution: | 1 (1.National Institutes for Food and Drug Control,Beijing 100050,China;2.Jilin City Institute for Drug Control,Jilin 132000,China; 3.Suzhou City Institute for Drug Control,Suzhou 215002,China) |
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| Abstract: | Objective:To identify the pigments or dyes,and establish analysis method for Croci Stigma adulteration.Methods: Using LC-MS method and comparing with the reference regents,to identify the main pigments and dyes.TLC and HPLC analytical methods were used for analysis of Croci Stigma adulteration.Results: Tartrazine,brilliant ponceau,auramine O and new fuchsin were identified as the main pigments and dyes.The results show that the above 4 pigments and dyes could be detected in 32 of totally 43 samples.Conclusion: The established method is able to detect the Croci Stigma adulteration quickly and effectively. |
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| Keywords: | Croci Stigma adulteration TLC HPLC LC-MS tartrazine brilliant ponceau auramine O new fuchsin TCM dyeing monitoring |
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