| HPLC法考察肌苷等4种对照品溶液的稳定性及不确定度分析 |
| |
| 引用本文： | 朱清丽,谭艳萍,柯红梅,孙全明,李宁.HPLC法考察肌苷等4种对照品溶液的稳定性及不确定度分析[J].西北药学杂志,2016(6):592-596. |
| |
| 作者姓名： | 朱清丽 谭艳萍 柯红梅 孙全明 李宁 |
| |
| 作者单位： | 安康市食品药品检验检测中心,安康,725000 |
| |
| 摘 要： | 目的考察被测对照品溶液的稳定性。方法用高效液相色谱法对肌苷、吡拉西坦、甲硝唑及曲安奈德4种对照品溶液进行稳定性考察,并采用不确定度对检测结果的准确性进行验证。结果肌苷对照品溶液使用期限为15d;吡拉西坦对照品溶液稳定性最好,使用期限为60d;甲硝唑对照品溶液较为稳定,使用期限为21d;曲安奈德对照品溶液稳定性较差,使用期限为7d。结论根据稳定性考察结果,为建立有效的质量控制方法提供参考。
|
| 关 键 词： | HPLC 对照品溶液 稳定性 不确定度 |
Study on the stability of control solutions of inosine,piracetam,metronidazole and triamcinolone acetonide by HPLC |
| |
| Abstract: | Objective To investigate the stability of 4 kinds of control solutions.Methods High performance liquid chromatography was used to study the stability and the accuracy uncertainty of inosine,derby of levetiracetam,metronidazole and triamcinolone acetonide control solutions,we investigated the stability.Results Inosine control solution could be used for a period of 1 5 days;pi-racetam for a period of 60 days;metronidazole reference solution was stable,and could be used for a period of 21 days;triamcin-olone acetonide reference solution stability was poor,could be used for a period of 7 days.Conclusion The results of the stability study supplied a reference for effective quality control. |
| |
| Keywords: | HPLC reference solution stability uncertainty degree |
| 本文献已被 万方数据 等数据库收录！ |
|
