| GC测定健儿清解液中6个挥发性成分的含量 |
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| 引用本文： | 冯美玲,毛菊华,刘敏,陈桂云,陈张金,吴查青.GC测定健儿清解液中6个挥发性成分的含量[J].中国现代应用药学,2020,37(13):1597-1601. |
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| 作者姓名： | 冯美玲 毛菊华 刘敏 陈桂云 陈张金 吴查青 |
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| 作者单位： | 丽水市食品药品与质量技术检验检测院,丽水市食品药品与质量技术检验检测院,丽水市食品药品与质量技术检验检测院,丽水市食品药品与质量技术检验检测院,丽水市食品药品与质量技术检验检测院,丽水市食品药品与质量技术检验检测院 |
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| 摘 要： | 目的 测定不同厂家生产的健儿清解液中挥发油成分糠醛、樟脑、苯甲醛、4-萜品醇、α-松油醇和龙脑的含量。方法 采用HP-INNOWAX毛细管柱为分离柱,以环己酮为内标,程序升温,进样口温度200 ℃,检测器：FID,温度220 ℃。结果 糠醛、樟脑、苯甲醛、4-萜品醇、α-松油醇和龙脑的线性范围分别为5.139～128.467 μg?ml-1(r=0.99990),1.900～47.500 μg?ml-1(r=0.99937),6.537～163.436 μg?ml-1(r=0.99996),1.057～26.423 μg?ml-1(r=0.99938),2.398～59.958 μg?ml-1(r=0.99923),1.014～25.346 μg?ml-1(r=0.99936)；该方法的回收率分别为97.0%,99.3%,98.6%,94.6%,93.5%,101.2%。不同厂家生产的健儿清解液中上述成分含量存在较大差别。结论 该方法可为健儿清解液质量标准的提高提供科学数据。
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| 关 键 词： | 健儿清解液 糠醛 樟脑 苯甲醛 4-萜品醇 α-松油醇 龙脑 |
| 收稿时间： | 2019/2/15 0:00:00 |
| 修稿时间： | 2019/6/17 0:00:00 |
Content Determination of Six Volatile Components in Jian'er Qingjie Solution by GC |
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| FENG Meiling,MAO Juhu,LIU Min,CHEN Guiyun,CHEN Zhangjin,WU Chaqing.Content Determination of Six Volatile Components in Jian'er Qingjie Solution by GC[J].The Chinese Journal of Modern Applied Pharmacy,2020,37(13):1597-1601. |
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| Authors: | FENG Meiling MAO Juhu LIU Min CHEN Guiyun CHEN Zhangjin WU Chaqing |
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| Institution: | Lishui Institute of Food and Drug & Quality and Technical Inspection,Lishui Institute of Food and Drug & Quality and Technical Inspection,Lishui Institute of Food and Drug & Quality and Technical Inspection,Lishui Institute of Food and Drug & Quality and Technical Inspection,Lishui Institute of Food and Drug & Quality and Technical Inspection,Lishui Institute of Food and Drug & Quality and Technical Inspection |
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