| 蒺藜全草中甾体皂苷类化学成分研究 |
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| 引用本文： | 吴克磊,康利平,熊呈琦,赵阳,余河水,张洁,马百平.蒺藜全草中甾体皂苷类化学成分研究[J].天津中医药大学学报,2012,31(4):225-228. |
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| 作者姓名： | 吴克磊 康利平 熊呈琦 赵阳 余河水 张洁 马百平 |
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| 作者单位： | 1. 100850 军事医学科学院放射与辐射医学研究所;300193 天津中医药大学
2. 100850,军事医学科学院放射与辐射医学研究所 |
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| 基金项目： | 北京市自然科学基金重大项目 |
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| 摘 要： | 目的]对蒺藜全草化学成分进行研究。方法]采用大孔吸附树脂柱色谱、硅胶柱色谱、ODS柱色谱及制备高效液相色谱法(PHPLC)对蒺藜70%乙醇提取液进行分离纯化,并利用理化数据测定和光谱数据分析等方法对所得单体进行了结构鉴定。结果]分离鉴定了5个甾体皂苷:1)uttroside B;2)polianthoside D;3)替告皂苷元-3-O-β-D-吡喃木糖基-(1→2)-β-D-吡喃木糖基-(1→3)]-β-D-吡喃葡糖基(1→4)-α-L-鼠李糖基(1→2)]-β-D-吡喃半乳糖苷;4)(25R)-26-O-β-D-吡喃葡糖基-5α-呋甾-3β,22α,26-三醇-3-O-β-D-吡喃葡萄糖基(1→4)-吡喃半乳糖苷;5)海柯皂苷元-3-O-β-D-吡喃葡萄糖基-(1→2)-β-D-吡喃木糖基-(1→3)]-β-D-吡喃葡萄糖基-(1→4)-β-D-吡喃半乳糖苷。结论]化合物1和2为首次从蒺藜中分离获得。
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| 关 键 词： | 蒺藜 甾体皂苷 分离纯化 结构鉴定 |
| 收稿时间： | 2012/9/29 0:00:00 |
Study on chemical components of Steroidal Saponins from Tribulus terrestris L. |
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| WU Ke-lei,KANG Li-ping,XIONG Cheng-qi,ZHAO Yang,YU He-shui,ZHANG Jie and MA Bai-ping.Study on chemical components of Steroidal Saponins from Tribulus terrestris L.[J].Journal of Tianjin University of Traditonal Chinese Medicine,2012,31(4):225-228. |
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| Authors: | WU Ke-lei KANG Li-ping XIONG Cheng-qi ZHAO Yang YU He-shui ZHANG Jie and MA Bai-ping |
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| Institution: | Institute of Radiation Medicine, Academy of Military Medical Sciences, Beijing 100850, China;Tianjin University of TCM, Tianjin 300193, China;Institute of Radiation Medicine, Academy of Military Medical Sciences, Beijing 100850, China;Tianjin University of TCM, Tianjin 300193, China;Institute of Radiation Medicine, Academy of Military Medical Sciences, Beijing 100850, China;Institute of Radiation Medicine, Academy of Military Medical Sciences, Beijing 100850, China;Institute of Radiation Medicine, Academy of Military Medical Sciences, Beijing 100850, China;Tianjin University of TCM, Tianjin 300193, China;Institute of Radiation Medicine, Academy of Military Medical Sciences, Beijing 100850, China;Institute of Radiation Medicine, Academy of Military Medical Sciences, Beijing 100850, China |
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| Abstract: | |
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| Keywords: | Tribulus terrestris L steroidal saponins isolation and purification structural elucidation |
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