| TLC、HPLC法测定清胃黄连丸中芍药苷、芒果苷含量 |
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| 引用本文： | 许明,宋新波,张丽娟,靳小慧,夏青,徐艳芬,习利平,程慧.TLC、HPLC法测定清胃黄连丸中芍药苷、芒果苷含量[J].辽宁中医学院学报,2011(11):227-229. |
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| 作者姓名： | 许明 宋新波 张丽娟 靳小慧 夏青 徐艳芬 习利平 程慧 |
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| 作者单位： | 天津中医药大学,天津300193 |
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| 摘 要： | 目的：对清胃黄连丸中芍药苷和芒果苷进行定性定量分析。方法：分别运用薄层色谱法和高效液相色谱法,对清胃黄连丸中所含的芍药苷和芒果苷进行测定。结果：对于方中所含的芍药苷和芒果苷,建立了薄层鉴定法,色谱斑点清晰,分离度良好,阴性无干扰;同时建立了高效液相色谱法,加样回收率分别为：芍药苷：RSD=2.71%,芒果苷：RSD=1.64%。结论：所建立的方法准确、简便、重复性好,可作为清胃黄连丸的质量标准的一个补充。
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| 关 键 词： | 清胃黄连丸 芍药苷 芒果苷 薄层色谱 高效液相色谱 |
Determination of Paeoniflorin and Mangiferin in Qingwei Huanglian Pill by TLC and HPLC |
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| Institution: | XU Ming,SONG Xin-bo,ZHANG Li-juan,JIN Xiao-hui,XIA Qing,XU Yan-feng,XI Li-ping,CHEN Hui(Tianjin University of Traditional Chinese Medicine,Tianjin 300193,China) |
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| Abstract: | Objective：To establish a method of qualitative and quantitative analysis of Paeoniflorin and mangiferin in Qingwei Huanglian Pills.Methods：TLC and HPLC were used for Paeoniflorin and mangiferin detection of Qingwei Huanglian Pills.Results：TLC can identify Paeoniflorin and mangiferin;HPLC can be used for content determination.The average recovery rate of Paeoniflorin：RSD=2.71%（n6）;The average recovery rate of mangiferin：RSD=1.64%（n=6）.Conclusion：The results demonstrated that the developed methods could be applied as an accurate simple and reliable quality standard for Qingwei Huanglian Pill. |
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| Keywords: | Qingwei Huanglian pills paeoniflorin mangiferin TLC HPLC |
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