| 妇炎克颗粒剂质量标准的研究 |
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| 引用本文： | 徐平声,石林阶.妇炎克颗粒剂质量标准的研究[J].湖南医科大学学报,2000,25(5):502-504. |
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| 作者姓名： | 徐平声 石林阶 |
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| 作者单位： | 附属湘雅医院药剂科,长沙 |
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| 摘 要： | 为制订妇炎克颗粒剂的质量标准，本文采用薄层色谱法对制剂中的黄柏、虎杖及甘草进行定性鉴别；并用薄层扫描法对制剂中盐酸小檗碱进行定量分析，结果表明盐酸小檗碱在０．４５７～３．２μｇ的浓度范围内具有良好的线性关系（ｒ＝０．９９９），加样回收率为９７．８６％，相对标准偏差ＲＳＤ为１．９６％。定性、定量方法简便、可靠、重现性好，具有实用性。
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| 关 键 词： | 妇炎克颗粒剂 薄层扫描法 质量标准 |
A study of quality standards for fuyanke granule] |
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| P S Xu,G S Tan,X Z Li.A study of quality standards for fuyanke granule][J].Bulletin of Hunan Medical University,2000,25(5):502-504. |
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| Authors: | P S Xu G S Tan X Z Li |
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| Institution: | Department of Pharmacy, Xiangya Hospital, Hunan Medical University, Changsha 410008. |
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| Abstract: | OBJECTIVE: To establish the quality standards for fuyanke(FYK) granule. METHODS: The phellodendron Chinese schneid, polygonum cuspidatum, sieb. et Zucc and glycyrrihza uralensis fisch in FYK granule were identified by thin-layer chromatography(TLC). The contents of berberine were determined by thin-layer chromatographic scanning(TLCs). RESULTS: The average recovery rate was 97.86%, and the relative standard deviation 1.96%. CONCLUSION: The method is simple, accurate and reliable. |
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