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| 中药红曲基原真菌的毛细管气相色谱法鉴别 | |
| 引用本文： | 邢旺兴,宓鹤鸣,陈斌,吴玉田,陈士景,贺祥.中药红曲基原真菌的毛细管气相色谱法鉴别[J].第二军医大学学报,2001,22(5):429-431. |
| 作者姓名： | 邢旺兴 宓鹤鸣 陈斌 吴玉田 陈士景 贺祥 |
| 作者单位： | 1. 第二军医大学药学院药物分析教研室, 2. 解放军第117医院, 3. 第二军医大学科研部 |
| 基金项目： | 国家中医药管理局重点课题基金资助项目 ( 97Z0 97) |
| 摘 要： | 目的：建立检测中药红曲基原菌中挥发性成分的毛细管气相色谱分析方法（CGC）。方法：采用毛细管气相色谱法分析紫色红曲霉系7种红曲栳瓣挥发性成分；进样口温度280℃，检测器温度280℃，程序升温条件：130℃，5min→10℃/min→200℃，10min，FID结果。结果：不同种红曲霉挥发性成分的种类和含量均存在显差异。根据红曲霉挥发性成分指纹图谱的主要峰及其相对含量，可以有效地鉴别红曲霉属真菌。结论：毛细0管气相色谱法对于鉴别红曲霉属真菌具有一定的实用价值。 |
| 关 键 词： | 红曲霉菌属 药物分析 中草药 气相色谱法 |
| 文章编号： | 0258-879X(2001)05-0429-03 |
| 修稿时间： | 2000年10月17日 |
Identifying the origin fungi of the traditional Chinese medicine Hongqu with capillary gas chromatography method |
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| XING Wang-xing,MI He-ming,CHEN Bin,CHEN Shi-Jing,HE Xiang,WU Yu-Tian.Identifying the origin fungi of the traditional Chinese medicine Hongqu with capillary gas chromatography method[J].Academic Journal of Second Military Medical University,2001,22(5):429-431. | |
| Authors: | XING Wang-xing MI He-ming CHEN Bin CHEN Shi-Jing HE Xiang WU Yu-Tian |
| Abstract: | Objective：To establish a capillary gas chromatography(CGC) method for identifying the origin fungi of traditional Chinese medicine Hongqu. Methods：The volatile components of 7 species of Monascus including M. purpureus Went, M.aurantiacus Lee, M. serorubesceus Sato, M. albidus Sato, M. barkeri Dangerd, M. ruber van Tieghem, and M.fuliginosus Sato were analyzed by capillary gas chromatography method. Inlet temperature and detector temperature were 280℃，temperature program were 130℃,5 min→10℃/min→200℃, 10 min FID was used for detection. Results：The variety and contents of the volatility components in Monascus had obvious differences which can be distinguished easily by the main fingerprint peaks within 20 min. Conclusion：This method is useful to identify of Monascus fungi. |
| Keywords: | Monascus pharmaceutical analysis drugs Chinese herbal chromatography gas |
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