| 气相色谱-质谱联用和光谱相关色谱法用于清肝注射液及茵陈药材中挥发性成分的相关分析 |
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| 引用本文： | 高海燕,郭方遒,易伦朝,梁逸曾.气相色谱-质谱联用和光谱相关色谱法用于清肝注射液及茵陈药材中挥发性成分的相关分析[J].时珍国医国药,2008,19(11). |
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| 作者姓名： | 高海燕 郭方遒 易伦朝 梁逸曾 |
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| 作者单位： | 中南大学化学化工学院中药现代化研究所,湖南,长沙,410083 |
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| 摘 要： | 目的对清肝注射液和茵陈药材中的挥发性成分进行定性、定量测定,并分析注射液和药材之间的相关性。方法采用气相色谱-质谱(GC-MS)法测定清肝注射液及茵陈药材中的挥发性成分并用光谱相关色谱法对它们之间的相关性进行分析。挥发性成分采用水蒸气蒸馏法提取。结果清肝注射液中分离出的23个主要物质,有21个来源于茵陈药材。茵陈药材中分离28个物质,定性25个。结论GC-MS法与光谱相关色谱法结合可对具有挥发性成分的中药注射液及其对应药材的相关性进行快速比较分析。
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| 关 键 词： | 清肝注射液 茵陈 气相色谱-质谱联用 光谱相关色谱 |
Analysis of Volatile Components in Qinggan Injection and Herbs Artemisiae Scopariae by GC- MS and Spectral Correlative Chromatography |
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| GAO Hai-yan,GUO Fang-qiu,YI Lun-zhao,LIANG Yi-zeng.Analysis of Volatile Components in Qinggan Injection and Herbs Artemisiae Scopariae by GC- MS and Spectral Correlative Chromatography[J].Lishizhen Medicine and Materia Medica Research,2008,19(11). |
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| Authors: | GAO Hai-yan GUO Fang-qiu YI Lun-zhao LIANG Yi-zeng |
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| Institution: | College of Chemistry and Chemical Engineering;Central South University;Changsha;410083;China |
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| Abstract: | Objective To detect and quantify the volatile components in Qinggan injection and Herba Artemisiae Scopariae and to find the sources of volatile components in Qinggan injection.Methods Volatile components extracted by hydro-distillation method in Qinggan injection and Herba Artemisiae Scopariae were analyzed by GC/MS.Spectral correlative chromatography method was applied to find their correlation.Results Twenty three components were isolated from Qinggan injection.21 of them could be found in Herba Artemisi... |
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| Keywords: | Qinggan injection Herba Artemisiae Scopariae GC/MS Spectral correlative chromatography |
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