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八角茴香药材质量标准研究
引用本文:袁经权,汪洋,周雅琴,周小雷,王硕,张蓉婷,闭春艳,覃玉宁,缪剑华.八角茴香药材质量标准研究[J].中华中医药杂志,2012(1):199-201.
作者姓名:袁经权  汪洋  周雅琴  周小雷  王硕  张蓉婷  闭春艳  覃玉宁  缪剑华
作者单位:广西药用植物研究所;桂林医学院
基金项目:国家科技攻关计划“西部开发”重大项目(No.2005BA901A09);广西科学研究与技术开发计划项目(No.桂科能10100027-3)~~
摘    要:目的:制定八角茴香的质量标准,为药用植物资源的开发利用提供科学依据。方法:采用定性鉴定方法和含量测定技术开展八角茴香药材质量标准研究。结果:对10个不同产地八角茴香的浸出物、总灰分和酸不溶灰分进行了测定;同时对其活性成分莽草酸和山柰酚进行了薄层定性鉴别,并对莽草酸进行了HPLC定量研究。结论:研究所得方法简便,准确,可有效控制八角茴香药材的质量。

关 键 词:八角茴香  质量标准  莽草酸  山柰酚  薄层色谱  高效液相色谱

Study on quality specification of Illiciun verum Hook.f.
YUAN Jing-quan,WANG Yang,ZHOU Ya-qin,ZHOU Xiao-lei,WANG Shuo,ZHANG Rong-ting,BI Chun-yan,QIN Yu-ning,MIAO Jian-hua.Study on quality specification of Illiciun verum Hook.f.[J].China Journal of Traditional Chinese Medicine and Pharmacy,2012(1):199-201.
Authors:YUAN Jing-quan  WANG Yang  ZHOU Ya-qin  ZHOU Xiao-lei  WANG Shuo  ZHANG Rong-ting  BI Chun-yan  QIN Yu-ning  MIAO Jian-hua
Institution:YUAN Jing-quan1,WANG Yang1,ZHOU Ya-qin1,ZHOU Xiao-lei1,WANG Shuo1,ZHANG Rong-ting1,BI Chun-yan2,QIN Yu-ning2,MIAO Jian-hua1(1Guangxi Medicinal Plant Research Institute,Nanning 530023,China;2Guiling Medical College,Guilin 561004,China)
Abstract:Objective: To provide scientific basis for the utilization and development of Illiciun verum by setting up the quality control specification.Method: The extract of I.verum was examined,ash was determined,and the bioactive constituents were analyzed by TLC and a HPLC analysis was applied for quatitative determination of shikimic acid.Result: Content of extract,total ash,and acid-insoluble ash of 10 samples from different habitats were determined.The qualitative and quantitative analysis of shikimic acid and kaempfetol by TLC and HPLC were also preformed respectively.Conclusion: The established method can be used for the quality control of Illiciun verum.
Keywords:Illiciun verum  Quality specification  Shikimic acid  Kaempfetol  TLC  HPLC
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