| 烘干与硫熏金银花药材HPLC指纹图谱对比 |
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| 引用本文： | 刘伟,茹凡书,崔永霞,韩永成.烘干与硫熏金银花药材HPLC指纹图谱对比[J].中国实验方剂学杂志,2013,19(4):111-113. |
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| 作者姓名： | 刘伟 茹凡书 崔永霞 韩永成 |
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| 作者单位： | 河南中医学院分析测试中心,郑州,450046 |
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| 基金项目： | 河南省教育厅自然科学研究计划项目(2010A360016) |
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| 摘 要： | 目的:建立不同产地烘干与硫熏金银花药材的指纹图谱,对比分析硫熏对金银花内在成分的影响.方法:采用高效液相色谱法,色谱条件:AichromBond-AQ C18色谱柱(4.6 mm×250 mm,5μm),流动相乙腈-0.1％磷酸水,梯度洗脱,流速1.0 mL· min-,柱温30℃,检测波长238 nm.结果:在选定的色谱条件下确定了20个共有峰构成10批烘干金银花药材的指纹特征指纹图谱,各批样品的相似度均＞0.96；16个共有峰构成10批硫熏金银花药材的指纹特征指纹图谱,各批样品的相似度均＞0.90.结论:该法精密度高、重复性好,可为烘干和硫熏金银花药材的指纹图谱评价提供依据.
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| 关 键 词： | 金银花 烘干 硫熏 高效液相色谱法 指纹图谱 |
| 收稿时间： | 2012/8/21 0:00:00 |
Comparison on Fingerprints of Drying and Sulphur Fumigated Lonicera japonica by HPLC |
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| LIU Wei,RU Fan-shu,CUI Yong-xia and HAN Yong-cheng.Comparison on Fingerprints of Drying and Sulphur Fumigated Lonicera japonica by HPLC[J].China Journal of Experimental Traditional Medical Formulae,2013,19(4):111-113. |
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| Authors: | LIU Wei RU Fan-shu CUI Yong-xia and HAN Yong-cheng |
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| Institution: | Center of Analysis and Measurement of Henan College of Traditional Chinese Medicine, Zhengzhou 450046, China;Center of Analysis and Measurement of Henan College of Traditional Chinese Medicine, Zhengzhou 450046, China;Center of Analysis and Measurement of Henan College of Traditional Chinese Medicine, Zhengzhou 450046, China;Center of Analysis and Measurement of Henan College of Traditional Chinese Medicine, Zhengzhou 450046, China |
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| Abstract: | |
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| Keywords: | Lonicera japonica drying sulphur fumigated HPLC fingerprints |
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