| 安息香化学成分研究 |
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| 引用本文： | 王峰,方振峰.安息香化学成分研究[J].中国实验方剂学杂志,2012,18(17):89-92. |
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| 作者姓名： | 王峰 方振峰 |
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| 作者单位： | 1. 广东药学院中药学院中药化学与分析系,广州,510006
2. 武汉生物工程学院制药工程系,武汉,430415 |
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| 基金项目： | 广东省高等学校高层次人才项目(2007ZYX04) |
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| 摘 要： | 目的:研究安息香95％乙醇提取物的化学成分.方法:利用色谱方法对安息香化学成分进行分离纯化,根据理化性质和波谱数据鉴定化合物的结构.结果:从安息香95％乙醇提取物中分离得到11个化合物,分别鉴定为19α-羟基-3-氧代齐墩果-12-烯-28-酸(1),6β-羟基-3-氧代齐墩果-12-烯-28-酸(2),苏门答腊树脂酸(3),泰国树脂酸(4),齐墩果酸(5),4-( E)-3-乙氧基丙-1-烯基]-2-甲氧基苯酚(6),苯甲酸(7),香草醛(8),香草酸(9),松柏醛(10),去氢双香草醛(11).结论:除苯甲酸外,其他化合物均为首次从该植物中分离得到.
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| 关 键 词： | 安息香 化学成分 三萜 |
| 收稿时间： | 2012/4/23 0:00:00 |
Chemical Constituents from Resin of Styrax tonkinensis |
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| WANG Feng and FANG Zhen-feng.Chemical Constituents from Resin of Styrax tonkinensis[J].China Journal of Experimental Traditional Medical Formulae,2012,18(17):89-92. |
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| Authors: | WANG Feng and FANG Zhen-feng |
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| Institution: | Department of Chinese Medicinal Chemistry and Analysis, School of Traditional Chinese Materia Medica, Guangdong Pharmaceutical University, Guangzhou 510006, China;Department of Pharmaceultical Engineering, Wuhan Bioegineering Institute, Wuhan 430415, China |
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| Abstract: | Objective:To investigate the chemical components of Styrax tonkinensis.Method: Chromatographic technologies were used for separation and purification,while physicochemical properties and spectral analysis were used for structure elucidation.Result: Eleven compounds were isolated and their structures were identified as 19α-hydroxy-3-oxo-olean-12-en-28-oic acid(1),6β-hydroxy-3-oxo-olean-12-en-28-oic acid(2),sumaresinolic acid(3),siaresinolic acid(4),oleanolic acid(5),4-(E)-3-ethoxyprop-1-enyl]-2-methoxyphenol(6),benzoic acid(7),vanillin(8),vanillic acid(9),coniferyl aldehyde(10),dehydrodivanillin(11).Conclusion: Except for compound 7,the other compounds were isolated from S.tonkinensis for the first time. |
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| Keywords: | Styrax tonkinensis chemical constituents triterpenoids |
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