| UPLC-ESI-MS-MS分析生晒参和紫红参中皂苷类成分 |
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| 引用本文： | 邱楠楠,刘金平,苏航,董刚,刘海燕,李平亚.UPLC-ESI-MS-MS分析生晒参和紫红参中皂苷类成分[J].中国实验方剂学杂志,2013,19(13):91-93. |
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| 作者姓名： | 邱楠楠 刘金平 苏航 董刚 刘海燕 李平亚 |
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| 作者单位： | 吉林大学再生医学科学研究所,长春,130021 |
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| 基金项目： | 吉林省科技厅重大项目(20096039) |
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| 摘 要： | 目的:采用UPLC-ESI-MS-MS方法比较生晒参和紫红参中人参皂苷类成分的种类及含量,阐明紫红参特异成分.方法:Waters ACQUITY UPLC BEH C18(2.1 mm× 50 mm,1.7 μm)色谱柱,流动相A(0.1％甲酸)-B(乙腈)梯度洗脱,柱温30℃；质谱条件:电喷雾离子化源(ESI),负离子检测模式.结果:与生晒参相比,紫红参中人参皂苷的种类和数量发生了改变,检测出含量较高的人参皂苷为20(S)-人参皂苷Rg3、20(R)-人参皂苷Rg3、20(R)-人参皂苷Rh1、20(R)-人参皂苷Rg2,Rk1,Rg5,Rd,Ro、姜状三七苷R1等.结论:人参加工成紫红参后皂苷类成分发生较大的变化,产生了大量稀有皂苷,人参加工可能产生紫红参的特异成分.
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| 关 键 词： | 生晒参 紫红参 人参皂苷 超高液相色谱-电喷雾-串联四级杆质谱联用仪 |
| 收稿时间： | 2012/9/27 0:00:00 |
Analysis on Ginsenosides of Dry Radix Ginseng and Purplish Red Ginseng with UPLC-MS-MS |
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| QIU Nan-nan,LIU Jin-ping,SU Hang,DONG Gang,LIU Hai-yan and LI Ping-ya.Analysis on Ginsenosides of Dry Radix Ginseng and Purplish Red Ginseng with UPLC-MS-MS[J].China Journal of Experimental Traditional Medical Formulae,2013,19(13):91-93. |
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| Authors: | QIU Nan-nan LIU Jin-ping SU Hang DONG Gang LIU Hai-yan and LI Ping-ya |
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| Institution: | Institute of Frontier Medical Science of Jilin University,Changchun 130021, China;Institute of Frontier Medical Science of Jilin University,Changchun 130021, China;Institute of Frontier Medical Science of Jilin University,Changchun 130021, China;Institute of Frontier Medical Science of Jilin University,Changchun 130021, China;Institute of Frontier Medical Science of Jilin University,Changchun 130021, China;Institute of Frontier Medical Science of Jilin University,Changchun 130021, China |
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| Abstract: | |
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| Keywords: | dry Radix Ginseng purplish red ginseng ginsenoside UPLC-ESI-MS/MS |
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