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淮阳金花菜脂溶性成分分析
引用本文:彭娟,马伯艳,范斌,闫寒,李杨,聂颖兰,孙健,刘长喜.淮阳金花菜脂溶性成分分析[J].中国实验方剂学杂志,2016,22(21):55-58.
作者姓名:彭娟  马伯艳  范斌  闫寒  李杨  聂颖兰  孙健  刘长喜
作者单位:北京市中医药防治重大疾病基础研究重点实验室, "道地药材国家重点实验室"培育基地, 中国中医科学院 医学实验中心, 北京 100700,黑龙江中医药大学 基础医学院, 哈尔滨 150040,北京市中医药防治重大疾病基础研究重点实验室, "道地药材国家重点实验室"培育基地, 中国中医科学院 医学实验中心, 北京 100700,北京市中医药防治重大疾病基础研究重点实验室, "道地药材国家重点实验室"培育基地, 中国中医科学院 医学实验中心, 北京 100700,北京市中医药防治重大疾病基础研究重点实验室, "道地药材国家重点实验室"培育基地, 中国中医科学院 医学实验中心, 北京 100700,北京市中医药防治重大疾病基础研究重点实验室, "道地药材国家重点实验室"培育基地, 中国中医科学院 医学实验中心, 北京 100700,北京市中医药防治重大疾病基础研究重点实验室, "道地药材国家重点实验室"培育基地, 中国中医科学院 医学实验中心, 北京 100700,北京中医药大学 养生学研究所, 北京 100029
基金项目:中央本级重大增减支项目(2060302)
摘    要:目的:探讨淮阳金花菜(秧草)脂溶性成分的组成。方法:石油醚提取秧草脂溶性成分,用气相色谱-质谱联用(GC-MS)法进行定性分析,鉴定其化学成分,并归一化法测定其相对含量。对其中的脂肪酸成分甲酯化,以正十七烷酸甲酯为内标对α-亚麻酸及棕榈酸进行了定量分析。结果:定性分析共检出26个色谱峰,鉴定出17个化合物,其中α-亚麻酸和棕榈酸占到了相对质量分数的45%。定量分析表明α-亚麻酸和棕榈酸的质量分数分别为0.62%,0.19%。结论:气相-质谱联用技术能够有效地分析秧草中脂溶性成分,秧草脂溶性成分中有益脂肪酸亚麻酸几乎为棕榈酸的3倍。以脂肪酸类化合物的现代研究结果阐明药食两用植物的营养价值,为其开发和利用提供更有力的依据。

关 键 词:淮阳金花菜  脂肪酸  气相色谱-质谱法
收稿时间:3/2/2016 12:00:00 AM

Analysis on Liposoluble Compounds of Huaiyang Medicago polymorpha
PENG Juan,MA Bo-yan,FAN Bin,YAN Han,LI Yang,NIE Ying-lan,SUN Jian and LIU Chang-xi.Analysis on Liposoluble Compounds of Huaiyang Medicago polymorpha[J].China Journal of Experimental Traditional Medical Formulae,2016,22(21):55-58.
Authors:PENG Juan  MA Bo-yan  FAN Bin  YAN Han  LI Yang  NIE Ying-lan  SUN Jian and LIU Chang-xi
Institution:Beijing Key Laboratory of Traditional Chinese Medicine Basic Research on Prevention and Treatment of Major Disease, the Cultivating Bases of the National Key Laboratory of Geo-Authentic Crude Drug, Experimental Research Center, China Academy of Chinese Medical Sciences, Beijing 100700, China,College of Basic Medicine, Heilongjiang University of Chinese Medicine, Harbin 150040, China,Beijing Key Laboratory of Traditional Chinese Medicine Basic Research on Prevention and Treatment of Major Disease, the Cultivating Bases of the National Key Laboratory of Geo-Authentic Crude Drug, Experimental Research Center, China Academy of Chinese Medical Sciences, Beijing 100700, China,Beijing Key Laboratory of Traditional Chinese Medicine Basic Research on Prevention and Treatment of Major Disease, the Cultivating Bases of the National Key Laboratory of Geo-Authentic Crude Drug, Experimental Research Center, China Academy of Chinese Medical Sciences, Beijing 100700, China,Beijing Key Laboratory of Traditional Chinese Medicine Basic Research on Prevention and Treatment of Major Disease, the Cultivating Bases of the National Key Laboratory of Geo-Authentic Crude Drug, Experimental Research Center, China Academy of Chinese Medical Sciences, Beijing 100700, China,Beijing Key Laboratory of Traditional Chinese Medicine Basic Research on Prevention and Treatment of Major Disease, the Cultivating Bases of the National Key Laboratory of Geo-Authentic Crude Drug, Experimental Research Center, China Academy of Chinese Medical Sciences, Beijing 100700, China,Beijing Key Laboratory of Traditional Chinese Medicine Basic Research on Prevention and Treatment of Major Disease, the Cultivating Bases of the National Key Laboratory of Geo-Authentic Crude Drug, Experimental Research Center, China Academy of Chinese Medical Sciences, Beijing 100700, China and Health Preservation Institute, Beijing University of Chinese Medicine, Beijing 100029, China
Abstract:
Keywords:Huaiyang Medicago polymorpha  fatty acid  chromatography-mass spectrometry (GC/MS)
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