| 川乌高压蒸制工艺优选 |
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| 引用本文： | 邓广海,林华.川乌高压蒸制工艺优选[J].中国实验方剂学杂志,2011,17(2):21-24. |
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| 作者姓名： | 邓广海 林华 |
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| 作者单位： | 1. 广州中医药大学,广州,510405
2. 广东省中医院药学部,广州,510120 |
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| 基金项目： | 广东省科技厅(2009B030801300) |
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| 摘 要： | 目的:优选川乌高压蒸制的工艺参数。方法:采用正交试验法考察蒸制时间、蒸制压力及处理方式等因素,以双酯型生物碱、总生物碱的含量及炮制品的外观评分为指标,综合优选川乌高压蒸制的最佳工艺。结果:川乌高压蒸制的最佳工艺为:A5B3C3,即川乌润湿后,于1.5 kg·cm-2压力下蒸制150 min。结论:该方法简单、可行而且易于控制,可作为代替川乌传统炮制工艺的新方法。
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| 关 键 词： | 川乌 双酯型生物碱 总生物碱 高压蒸制 正交设计 HPLC |
| 收稿时间： | 2010/9/11 0:00:00 |
Orthogonal Test for Optimizing Processing Technology under High-Pressure of Radix Aconiti |
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| DENG Guang-hai and LIN Hua.Orthogonal Test for Optimizing Processing Technology under High-Pressure of Radix Aconiti[J].China Journal of Experimental Traditional Medical Formulae,2011,17(2):21-24. |
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| Authors: | DENG Guang-hai and LIN Hua |
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| Institution: | DENG Guang-hai1,LIN Hua2(1.Guangzhou University of Traditional Chinese Medicine,Guangzhou 510405,China,2.Department of Pharmacy,Guangdong Provincial Hospital of Traditional Chinese Medicine,Guangzhou 510120,China) |
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| Abstract: | Objective:To optimize the best method of processing Radix Aconiti under high-pressure.Method:Orthogonal test was used to study the effect of three factors including processing time,processing pressure and processing mode.The content of di-ester alkaloids and total alkaloids was determined as the investigative index,at the same time,properties of process was evaluated by the grading methods of synthesizing multiple guidelines to optimize the best method of processing Radix Aconiti under high-pressure.Result:... |
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| Keywords: | Radix Aconiti di-ester alkaloids total alkaloids processing under high-pressure orthogonal design HPLC |
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