| HPLC测定木香槟榔丸中 木香烃内酯和去氢木香内酯的含量 |
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| 引用本文： | 鞠成国,王巍,高慧,史辑.HPLC测定木香槟榔丸中 木香烃内酯和去氢木香内酯的含量[J].中国实验方剂学杂志,2011,17(23):74-76. |
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| 作者姓名： | 鞠成国 王巍 高慧 史辑 |
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| 作者单位： | 辽宁中医药大学药学院,辽宁大连,116600 |
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| 摘 要： | 目的:建立木香槟榔丸中木香烃内酯和去氢木香内酯的含量测定方法。方法:采用HPLC,色谱柱为Agilent C18(4.6 mm×250 mm,5μm),流动相甲醇-水(65∶35),检测波长225 nm,柱温30℃,流速1.0 mL.min-1。结果:木香烃内酯和去氢木香内酯的线性范围分别为0.046 4～0.3 712μg(r=0.999 6)和0.045 2～0.361 6μg(r=0.999 5);平均加样回收率分别为99.0%(RSD 0.86%,n=6)和99.2%(RSD 0.23%,n=6)。结论:该法简便,快速,结果准确,重复性好,可用于控制木香槟榔丸的质量。
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| 关 键 词： | 木香槟榔丸 木香烃内酯 去氢木香内酯 高效液相色谱法 |
| 收稿时间： | 2011/2/18 0:00:00 |
Determination of Costunolide and Dehydrocostus Lactone in Muxiangbinglang Pill by HPLC |
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| JU Cheng-guo,WANG Wei,GAO Hui and SHI Ji.Determination of Costunolide and Dehydrocostus Lactone in Muxiangbinglang Pill by HPLC[J].China Journal of Experimental Traditional Medical Formulae,2011,17(23):74-76. |
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| Authors: | JU Cheng-guo WANG Wei GAO Hui and SHI Ji |
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| Institution: | School of Pharmacy, Liaoning University of Traditional Chinese Medicine, Dalian 116600, China;School of Pharmacy, Liaoning University of Traditional Chinese Medicine, Dalian 116600, China;School of Pharmacy, Liaoning University of Traditional Chinese Medicine, Dalian 116600, China;School of Pharmacy, Liaoning University of Traditional Chinese Medicine, Dalian 116600, China |
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| Abstract: | |
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| Keywords: | Muxiangbinglang pill costunolide dehydrocostus lactone HPLC |
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