| 不同硫磺熏蒸程度白芷二氧化硫残留量与有效成分含量的相关性 |
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| 引用本文： | 卢晓琳,马逾英,张福卓,宗露,蒋运斌.不同硫磺熏蒸程度白芷二氧化硫残留量与有效成分含量的相关性[J].中国实验方剂学杂志,2013,19(9):139-142. |
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| 作者姓名： | 卢晓琳 马逾英 张福卓 宗露 蒋运斌 |
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| 作者单位： | 成都中医药大学药学院中药资源系统研究与开发利用省部共建国家重点实验室培育基地,成都,611137 |
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| 基金项目： | 国家"十一五"科技支撑计划(2007BAI40B02) |
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| 摘 要： | 目的:探讨经硫磺熏蒸后白芷的二氧化硫残留量与有效成分欧前胡素和氧化前胡素含量的相关性,为制订其科学合理、客观可控的二氧化硫限量标准提供科学依据.方法:采用《中国药典》2010年版附录方法进行二氧化硫残留量的动态检测;采用课题组前期建立的HPLC对不同硫磺熏蒸程度的白芷进行欧前胡素和氧化前胡素的含量测定;采用曲线回归的方法进行二氧化硫残留量与有效成分含量的关联分析.结果:自然晒干的白芷样品其二氧化硫残留量低于其他经过硫磺熏蒸的样品,氧化前胡素和欧前胡素均高于其他经过硫磺熏蒸的样品.随着硫磺用量和熏蒸时间的增加,二氧化硫残留量升高,氧化前胡素和欧前胡素的含量下降,且二者随着二氧化硫残留量增加而降低.结论:初步探讨了随着硫磺熏蒸程度的增加,二氧化硫残留量、有效成分含量的变化规律,为下一步的深入研究提供参考.
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| 关 键 词： | 白芷 硫磺熏蒸 二氧化硫残留量 欧前胡素 氧化前胡素 |
| 收稿时间： | 2012/11/24 0:00:00 |
Correlation between Residues (SO2) and Chemical Contents of Angelica Dahurica Radix in Different Sulfur-fumigated Degree |
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| LU Xiao-lin,MA Yu-ying,ZHANG Fu-zhuo,ZONG Lu and JIANG Yun-bin.Correlation between Residues (SO2) and Chemical Contents of Angelica Dahurica Radix in Different Sulfur-fumigated Degree[J].China Journal of Experimental Traditional Medical Formulae,2013,19(9):139-142. |
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| Authors: | LU Xiao-lin MA Yu-ying ZHANG Fu-zhuo ZONG Lu and JIANG Yun-bin |
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| Institution: | School of Pharmacy, Chengdu University of Traditional Chinese Medicine, State Key Laboratory Breeding Base of Systematic Research, Development and Utilization of Chinese Medicine Resources, Chengdu 611137, China;School of Pharmacy, Chengdu University of Traditional Chinese Medicine, State Key Laboratory Breeding Base of Systematic Research, Development and Utilization of Chinese Medicine Resources, Chengdu 611137, China;School of Pharmacy, Chengdu University of Traditional Chinese Medicine, State Key Laboratory Breeding Base of Systematic Research, Development and Utilization of Chinese Medicine Resources, Chengdu 611137, China;School of Pharmacy, Chengdu University of Traditional Chinese Medicine, State Key Laboratory Breeding Base of Systematic Research, Development and Utilization of Chinese Medicine Resources, Chengdu 611137, China;School of Pharmacy, Chengdu University of Traditional Chinese Medicine, State Key Laboratory Breeding Base of Systematic Research, Development and Utilization of Chinese Medicine Resources, Chengdu 611137, China |
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| Abstract: | |
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| Keywords: | Angelica Dahurica Radix sulfur fumigation sulfur dioxide residues imperatorin oxypeucedanin |
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