| 乌骨藤总苷H的化学成分研究 |
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| 引用本文： | 沈利君,周建设,李晓誉,陈金文.乌骨藤总苷H的化学成分研究[J].中国药学杂志,2011,46(8):585-588. |
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| 作者姓名： | 沈利君 周建设 李晓誉 陈金文 |
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| 作者单位： | 浙江省杭州市萧山区第一人民医院;浙江省医学科学院; |
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| 摘 要： | 目的 研究乌骨藤总苷H的化学成分。方法 采用柱色谱和HPLC技术对乌骨藤总苷H中的化学成分进行分离纯化，并通过理化性质和波谱方法鉴定其结构。结果 从骨藤总苷H中分离得到6个化合物，分别鉴定为tenacissoside A(1、tenacissoside B(2、tenacissoside C(3、tenacissoside D(4、marsdenoside K(5、11-α-O-乙酰基-12-β-O-惕各酰基tenacigenin B 3-O-β-D-葡萄吡喃糖基-(1→4-6-去氧-3-O-甲基-β-D-阿洛吡喃糖基-(1→4-β-D-夹竹桃吡喃糖苷(6。结论 化合物6是新化合物，为首次从该属植物中分离得到。
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| 关 键 词： | 乌骨藤 11-α-O-乙酰基-12-β-O-惕各酰基tenacigenin B 3-O-β-D-葡萄吡喃糖基-(1→4-6-去氧-3-O-甲基-β-D-阿洛吡喃糖基-(1→4-β-D-夹竹桃吡喃糖苷 化学成分 |
| 收稿时间： | 2011-11-11; |
Study on the Chemical Constituents of Total Glycoside H of Marsdenia tenacissima |
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| SHEN Li-jun,ZHOU Jian-she,LI Xiao-yu,CHEN Jin-wen.Study on the Chemical Constituents of Total Glycoside H of Marsdenia tenacissima[J].Chinese Pharmaceutical Journal,2011,46(8):585-588. |
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| Authors: | SHEN Li-jun ZHOU Jian-she LI Xiao-yu CHEN Jin-wen |
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| Institution: | SHEN Li-jun1,ZHOU Jian-she1,LI Xiao-yu2,CHEN Jin-wen1(1.The First People's Hospital of Xiaoshan,Hangzhou 311201,China,2.Zhejiang Academy of Medical Sciences,Hangzhou 310012,China) |
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| Abstract: | OBJECTIVE To investigate the chemical constituents of the total glycoside H of Marsdenia tenacissima. METHODS The compounds were isolated and purified by column chromatography and HPLC. Their structures were identified by the physicochemical characteristics and spectroscopic analyses. RESULTS Six compounds were isolated from total glycoside H of Marsdenia tenacissima， and their structures were identified as tenacissoside A(1， tenacissoside B(2， tenacissoside C(3， tenacissoside D(4， marsdenoside K(5， 11-α-O-ethanoyl-12-β-O-tigloxyl tenacigenin B 3-O-β-D-glucopyranosyl-(1→4-6-deoxy-3-O-methyl-β-D-allopyranosyl-(1→4-β-D-oleandropyranoside(6. CONCLUSION Compound 6 was isolated from this plant for the first time. |
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| Keywords: | Marsdenia tenacissima" target="_blank">Marsdenia tenacissima')" href="#">Marsdenia tenacissima 11-α-O-ethanoyl-12-β-O-tigloxyl tenacigenin B 3-O-β-D-glucopyranosyl-(1→4-6-deoxy-3-O-methyl-β-D-allopyranosyl-(1→4-β-D-oleandropyranoside" target="_blank">α-O-ethanoyl-12-β-O-tigloxyl tenacigenin B 3-O-β-D-glucopyranosyl-(1→4-6-deoxy-3-O-methyl-β-D-allopyranosyl-(1→4-β-D-oleandropyranoside')" href="#">11-α-O-ethanoyl-12-β-O-tigloxyl tenacigenin B 3-O-β-D-glucopyranosyl-(1→4-6-deoxy-3-O-methyl-β-D-allopyranosyl-(1→4-β-D-oleandropyranoside chemical constituents |
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