| 中药吴茱萸RP-HPLC指纹图谱的研究 |
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| 引用本文： | 洪玉梅,蔡嵩,高慧敏,王维皓,王智民.中药吴茱萸RP-HPLC指纹图谱的研究[J].中国药学杂志,2006,41(12):895-898. |
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| 作者姓名： | 洪玉梅 蔡嵩 高慧敏 王维皓 王智民 |
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| 作者单位： | 中国中医科学院中药研究所,北京,100700 |
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| 摘 要： | 目的建立吴茱萸饮片的RP-HPLC指纹图谱研究方法。方法Alltech C18色谱柱;梯度洗脱;流速:1.0 mL·min-1;检测波长:254 nm;柱温:40℃。结果该方法具有良好的稳定性和重复性,19个产地吴茱萸饮片及其炮制品共标定了15个共有峰。结论利用吴茱萸RP-HPLC指纹图谱分析法可较全面的反映吴茱萸饮片的内在质量,可用于吴茱萸饮片的质量控制。
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| 关 键 词： | 吴茱萸 指纹图谱 |
| 文章编号： | 1001-2494（2006）12-0895-04 |
| 收稿时间： | 2005-05-25 |
| 修稿时间： | 2005-05-25 |
Study on RP-HPLC Fingerprint of Fructus evodiae |
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| HONG Yu-mei,CAI Song,GAO Hui-min,WANG Wei-hao,WANG Zhi-min.Study on RP-HPLC Fingerprint of Fructus evodiae[J].Chinese Pharmaceutical Journal,2006,41(12):895-898. |
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| Authors: | HONG Yu-mei CAI Song GAO Hui-min WANG Wei-hao WANG Zhi-min |
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| Institution: | Institute of Chinese Materia Medica， China Academy of Traditional Chinese Medicine， Beijing 100700， China |
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| Abstract: | OBJECTIVE To determine the RP-HPLC fingerprint of Fructus evodiae.METHODS The separation was performed on an Alltech C18 column with gradient elution.The flow rate was 1.0 mL·min-1.UV detecting wavelength was at 254 nm,and column temperature was at 40 ℃.RESULTS Fifteen same peaks in the HPLC profile were found in the fruits of Fructus evodiae planted from 19 different places.The method is simple and accurate with good reproducibility.CONCLUSION The RPHPLC fingerprint is used to control the quality of Fructus evodiae. |
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| Keywords: | Fructus evodiae fingerprint |
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