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GC-MS分析栀子姜制前后挥发油的化学组成成分变化
引用本文:李雨田,肖永庆,张村,于定荣,麻印莲,顾雪竹.GC-MS分析栀子姜制前后挥发油的化学组成成分变化[J].中国中药杂志,2011,36(24):3434-3438.
作者姓名:李雨田  肖永庆  张村  于定荣  麻印莲  顾雪竹
作者单位:中国中医科学院中药研究所,北京,100700
基金项目:国家"重大新药创制"科技重大专项(2009ZX09301);中国中医科学院自主选题项目(ZZ20090110)
摘    要:目的:比较栀子姜制前后挥发油中的化学成分在组成和含量 上的变化,为阐释姜栀子配伍炮制的物质基础内涵提供科学依据.方法:采用水蒸气蒸馏法提取栀子、生姜、姜栀子中的挥发油,利用GC-MS鉴定并比较分析3个样品中化学成分变化,应用峰面积归一化法计算各成分的相对质量分数.结果:栀子、生姜、姜栀子挥发油的质量分数分别为1.0,2.0,1.5μL·g-1.从栀子、生姜和姜栀子挥发油中分别检出42,75,77个色谱峰,总共鉴定了89种化合物,其中栀子30种、生姜58种、姜栀子67种,分别占挥发油总量的94.10%,90.52%,94.38%.结论:栀子姜制后挥发油成分在含量和组成上均发生了明显变化.

关 键 词:栀子  生姜  姜栀子  挥发油  GC-MS
收稿时间:2011/6/21 0:00:00

Analysis of volatile oil in Gardenia jasminoids roasted with ginger juice by GC-MS
LI Yutian,XIAO Yongqing,ZHANG Cun,YU Dingrong,MA Yinlian and GU Xuezhu.Analysis of volatile oil in Gardenia jasminoids roasted with ginger juice by GC-MS[J].China Journal of Chinese Materia Medica,2011,36(24):3434-3438.
Authors:LI Yutian  XIAO Yongqing  ZHANG Cun  YU Dingrong  MA Yinlian and GU Xuezhu
Institution:LI Yutian,XIAO Yongqing,ZHANG Cun,YU Dingrong,MA Yinlian,GU Xuezhu (Institute of Chinese Materia Medica,China Academy of Chinese Medical Sciences,Beijing 100700,China)
Abstract:Objective: To compare the components and contents of volatile oil in Gardenia jasminoids,Zingiber officinale,G.jasminoids roasted with ginger juice and to provide scientific basis for intrinsic material of G.jasminoids roasted with ginger juice.Method: The volatile oil in the three herbal medicines was extracted by steam distillation,the components were analyzed by GC-MS and the contents of the components were calculated by area normalization method.Result: The contents of volatile oil in G.jasminoids,Z.off...
Keywords:Gardenia jasminoids  Zingiber officinale  Gardenia jasminoids roasted with ginger juice  volatile oil  GC-MS
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