| 山丹芍药汤化学成分的分离与鉴定(Ⅰ) |
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| 引用本文： | 文志明,徐礼燊.山丹芍药汤化学成分的分离与鉴定(Ⅰ)[J].中国中药杂志,2001,26(6):406-408. |
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| 作者姓名： | 文志明 徐礼燊 |
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| 作者单位： | 中国医学科学院中国协和医科大学药物研究所, |
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| 摘 要： | 目的 :对山丹芍药汤化学成分进行研究。方法 :水提醇沉法制备样品 ,氯仿、乙酸乙酯和水饱和正丁醇提取 ,硅胶、聚酰胺柱进行分离 ,物理、化学和光谱学方法鉴定化合物。结果和结论 :从氯仿和乙酸乙酯提取部分分得 6个化合物 ,为丹参酮ⅡA、苯甲酸、阿魏酸、隐丹参酮、β-谷甾醇和熊果酸。
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| 关 键 词： | 山丹芍药汤 化学成分 |
| 文章编号： | 1001-5302（2001）06-0406-03 |
| 收稿时间： | 2000/5/29 0:00:00 |
| 修稿时间： | 2000年5月29日 |
Isolation and Elucidation
of Chemical Constituents of Shandanshaoyao Decoction( |
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| WEN Zhi ming;XU Li xin.Isolation and Elucidation
of Chemical Constituents of Shandanshaoyao Decoction([J].China Journal of Chinese Materia Medica,2001,26(6):406-408. |
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| Authors: | WEN Zhi ming;XU Li xin |
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| Institution: | Institute of Materia Medica, Chinese Academy of Medical Sciences, Peking Union Medical College, Beijing 100050, China. |
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| Abstract: | OBJECTIVE: To study the chemical constituents of Shandanshaoyao Decoction. METHOD: The sample was prepared using boiling water, then precipitated by 75% ethanol. The ethanol soluble fraction was extracted by chloroform, ethyl acetate and n-butanol respectively. The extracts were isolated using silica gel and polyamide column chromatography, and the chemical constituents were identified by chemical and spectroscopic methods. RESULT: Six compounds were isolated from the chloroform and ethyl acetate extracts, and elucidated as tanshinone IIA, benzoic acid, ferulic acid, cryptotanshinone, beta-stitosterol and ursolic acid respectively. CONCLUSION: A preliminary study on the chemical constituents in traditional Chinese compound recipe Shandanshaoyao Decoction is reported. |
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| Keywords: | Shandanshaoyao Decoction chemical constituents |
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