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顶羽菊化学成分研究
引用本文:赵东保,张卫,李明静,刘绣华.顶羽菊化学成分研究[J].中国中药杂志,2006,31(22):1869-1872.
作者姓名:赵东保  张卫  李明静  刘绣华
作者单位:河南大学,化学化工学院,河南,开封,475001
摘    要:目的:研究顶羽菊Acroptilon repens的化学成分。方法:采用硅胶柱色谱法进行分离纯化,根据光谱数据进行结构鉴定。结果:从乙醇提取物中分离得到了11个化合物,分别鉴定为2α, 9β-二羟基去氢木香内酯(1),cynaropicrin(2),芹菜素(3),豆甾醇(4),4′-羟基汉黄芩素(5),咖啡酸乙酯(6),对甲氧基桂皮酸(7),木犀草素(8),胡萝卜苷(9),芹菜素-7-O-β-D-葡萄糖苷(10),丁香苷(11)。结论:化合物1为新化合物,化合物5~11系首次从该植物中分离得到。

关 键 词:顶羽菊  化学成分        9β-二羟基去氢木香内酯
文章编号:1001-5302(2006)22-1869-04
收稿时间:2006-06-19
修稿时间:2006-06-19

Studies on chemical constituents of Acroptilon repens
ZHAO Dong-bao;ZHANG Wei;Li Ming-jing;LIU Xiu-hua.Studies on chemical constituents of Acroptilon repens[J].China Journal of Chinese Materia Medica,2006,31(22):1869-1872.
Authors:ZHAO Dong-bao;ZHANG Wei;Li Ming-jing;LIU Xiu-hua
Institution:College of Chemistry and Chemical Engineering, Henan University, Kaifeng 475001, China
Abstract:OBJECTIVE: To investigate the chemical constituents of Acroptilon repens. METHOD: The ethanol extract of A. repens was isolated and purified by means of chromatography. These compounds were identified by their spectral data. RESULT: 11 compounds were isolated and identified as 2alpha, 9beta-dihydroxy-dehydrocostus lactone (1) , cynaropicrin (2) , apigenin (3) , stigmasterol (4) , 4' -hydroxywogonin (5) , ethyl caffeate (6) , p-methoxy-cinnamic acid (7) , luteolin (8) , daucosterol (9) , apigenin-7-O-beta-D-glucoside (10) , syringin (11). CONCLUSION: Compounds 5-11 were isolated from A. repens for the first time. Compound 1 is new compounds.
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