| 金银花的化学成分研究 |
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| 引用本文： | 王芳,蒋跃平,王晓良,林生,卜鹏滨,朱承根,王素娟,杨永春,石建功.金银花的化学成分研究[J].中国中药杂志,2013,38(9):1378-1385. |
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| 作者姓名： | 王芳 蒋跃平 王晓良 林生 卜鹏滨 朱承根 王素娟 杨永春 石建功 |
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| 作者单位： | 天然药物活性物质与功能国家重点实验室,中国医学科学院北京协和医学院药物研究所,北京100050 |
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| 基金项目： | 国家自然科学基金项目(20772156,30825044,20932007);国家"重大新药创制"科技重大专项(2009ZX09311-004) |
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| 摘 要： | 目的:通过正相硅胶、大孔吸附树脂、MCI树脂、Sephadex LH-20,制备薄层色谱和反相HPLC等多种色谱分离方法相结合,从金银花中分离得到18个化合物；借助波谱学分析方法鉴定它们的结构分别为:adinoside A(1),stryspinoside(2),苄醇β-D-吡喃葡萄糖苷(3),苄基-2-O-β-D-吡喃葡萄糖基-2,6-二羟基苯甲酸酯(4),2,5-二羟基苯甲酸-5-O-β-D-吡喃葡萄糖苷(5),丁香油酚-β-D-吡喃葡萄糖苷(6),丁香油酚-βD-吡喃木糖基-(1→6)-β-D-吡喃葡萄糖苷(7),(-)-南烛木树脂酚9-O-β-D-吡喃葡萄糖苷(8),(+)-南烛木树脂酚9-O-β-D-吡喃葡萄糖苷(9),芹菜素7-O-α-L-鼠李糖苷(10),木犀草素3’-O-L-鼠李糖苷(11),熊果酸(12),β-谷甾醇3-O-β-D-葡萄糖苷-6'-O-棕榈酸酯(13),脱落酸(14),鸟苷(15),5-甲氧基尿嘧啶(16),反式桂皮酸(17)和对羟基苯甲醛(18).以上化合物均为首次从金银花中分离得到.
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| 关 键 词： | 金银花 环烯醚萜苷 苄醇苷 酚苷 木脂素苷 黄酮苷 |
| 收稿时间： | 2/1/2013 12:00:00 AM |
Chemical constituents from flower buds of Lonicera japonica |
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| WANG Fang,JIANG Yue-ping,WANG Xiao-liang,LIN Sheng,PU Peng-bin,ZHU Cheng-gen,WANG Su-juan,YANG Yong-chun and SHI Jian-gong.Chemical constituents from flower buds of Lonicera japonica[J].China Journal of Chinese Materia Medica,2013,38(9):1378-1385. |
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| Authors: | WANG Fang JIANG Yue-ping WANG Xiao-liang LIN Sheng PU Peng-bin ZHU Cheng-gen WANG Su-juan YANG Yong-chun and SHI Jian-gong |
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| Institution: | Key Laboratory of Bioactive Substance and Function of Natural Medicines, Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, China;Key Laboratory of Bioactive Substance and Function of Natural Medicines, Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, China;Key Laboratory of Bioactive Substance and Function of Natural Medicines, Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, China;Key Laboratory of Bioactive Substance and Function of Natural Medicines, Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, China;Key Laboratory of Bioactive Substance and Function of Natural Medicines, Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, China;Key Laboratory of Bioactive Substance and Function of Natural Medicines, Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, China;Key Laboratory of Bioactive Substance and Function of Natural Medicines, Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, China;Key Laboratory of Bioactive Substance and Function of Natural Medicines, Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, China;Key Laboratory of Bioactive Substance and Function of Natural Medicines, Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, China |
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| Abstract: | |
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| Keywords: | Lonicera japonica iridoid glycosides benzyl glycoside phenolic glycosides lignin glycosides flavone glycosides |
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