| 小野芝麻化学成分的研究(Ⅰ) |
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| 引用本文： | 蒋受军,朱斌,魏锋,林瑞超,鲁静.小野芝麻化学成分的研究(Ⅰ)[J].中国中药杂志,2002,27(9):671-673. |
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| 作者姓名： | 蒋受军 朱斌 魏锋 林瑞超 鲁静 |
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| 作者单位： | 1. 广西壮族自治区药品检验所,广西南宁,530021
2. 中国药品生物制品检定所,北京,100050 |
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| 摘 要： | 目的 :对小野芝麻的化学成分进行了化学鉴定。方法 :采用色谱技术进行分离、纯化 ,利用FAB MS ,IR ,UV ,1 HNMR ,13 CNMR ,DEPT ,HMQC ,HMBC等手段及理化常数鉴定结构。结果 :分离得到 2个化合物 ,分别为芹菜素-7-O-β-D-(6′-对羟基肉桂酸基 ) 甘露糖苷 (I) ,毛蕊花糖苷 (Ⅱ)。结论 :化合物I为新化合物 ,化合物Ⅱ为首次从该植物中分离得到。
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| 关 键 词： | 小野芝麻 化学成分 小野芝麻苷 毛蕊花糖苷 |
| 文章编号： | 1001-5302(2002)09-0671-03 |
| 收稿时间： | 2001/11/3 0:00:00 |
| 修稿时间： | 2001年11月3日 |
Studies on the Chemical Constituents in Herba of Galeobdolon chinense (Ⅰ) |
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| JIANG Shou jun ;ZHU Bin ;WEI Feng ;LIN Rui chao ;LU Jing.Studies on the Chemical Constituents in Herba of Galeobdolon chinense (Ⅰ)[J].China Journal of Chinese Materia Medica,2002,27(9):671-673. |
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| Authors: | JIANG Shou jun ;ZHU Bin ;WEI Feng ;LIN Rui chao ;LU Jing |
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| Institution: | Guangxi Institute for the Drug Control, Nanning 530021, Guangxi, China. National Institute for the Control of Pharmaceutical and Biological Products, Beijing 100050, China. jiangshoujun@sina.com |
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| Abstract: | OBJECTIVE: To study the chemical constituents in the Galeobdolon chinense. METHOD: The chemical constituents were separated by means of chromatogrophy, and their structures were identified by spectra of FAB-MS, IR, UV, 1H-NMR, 13C-NMR, DEPT, HMQC and HMBC. RESULT: Two compounds were obtained and identified as galeobdoside (I) whose structure was apigenin-7-O-beta-D-(6'-p-hydoxy-cinnamoyloxy)-mannoside and verbascoside (II). CONCLUSION: Compound I was a new compound and compound II was obtained from this plant for the first time. |
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| Keywords: | Galeobdolon chinense chemical compoents galeobdoside verbascoside |
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