| 石菖蒲乙醇提取物石油醚部分化学成分的研究 |
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| 引用本文： | 朱梅菊,谭宁华,嵇长久,徐俊驹,贺文军,张玉梅.石菖蒲乙醇提取物石油醚部分化学成分的研究[J].中国中药杂志,2010,35(2):173-176. |
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| 作者姓名： | 朱梅菊 谭宁华 嵇长久 徐俊驹 贺文军 张玉梅 |
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| 作者单位： | 1. 中国科学院,昆明植物研究所,植物化学与西部植物资源持续利用国家重点实验室,云南,昆明,650204;湛江师范学院,体育科学学院,广东,湛江,524048
2. 中国科学院,昆明植物研究所,植物化学与西部植物资源持续利用国家重点实验室,云南,昆明,650204 |
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| 基金项目： | 国家杰出青年科学基金项目(30725048);广东省自然科学基金项目(31938);湛江市科技招标项目(湛科[2005]97号);中国科学院"西部之光"人才培养计划"联合学者"项目 |
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| 摘 要： | 目的:对石菖蒲乙醇提取物的石油醚部分进行化学成分研究.方法:采用柱色谱、重结晶等分离纯化化合物,应用EI-MS,NMR等波谱技术鉴定化合物结构.结果:从石菖蒲乙醇提取物石油醚萃取部分分得7个化合物,经波谱分析鉴定为1-hydroxy-7(11),9-guaiadien-8-one(1),菖蒲醇酮(2),α-细辛醚(3),1,8二羟基-3-甲基蒽醌(4),1,8-二羟基-3-甲氧基-6-甲基蒽醌(5),1,3,8-三羟基-6-甲基蒽醌(6),(+)-galbacin(7).结论:化合物l为新化合物,化合物4～7均为首次从该植物中分到.
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| 关 键 词： | 石菖蒲 倍半萜 化学成分 |
| 收稿时间： | 2009/7/14 0:00:00 |
Chemical constituents from petroleum ether fraction of ethanolextract of Acorus tatarinowii |
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| ZHU Meiju,TAN Ninghu,JI Changjiu,XU Junju,HE Wenjun and ZHANG Yumei.Chemical constituents from petroleum ether fraction of ethanolextract of Acorus tatarinowii[J].China Journal of Chinese Materia Medica,2010,35(2):173-176. |
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| Authors: | ZHU Meiju TAN Ninghu JI Changjiu XU Junju HE Wenjun and ZHANG Yumei |
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| Institution: | State Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute ofBotany, Chinese Academy of Sciences, Kunming 650204,China;Sports Science Institute, Zhanjiang Normal Univrsity, Zhanjiang 524048, China;State Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute ofBotany, Chinese Academy of Sciences, Kunming 650204,China;State Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute ofBotany, Chinese Academy of Sciences, Kunming 650204,China;State Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute ofBotany, Chinese Academy of Sciences, Kunming 650204,China;State Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute ofBotany, Chinese Academy of Sciences, Kunming 650204,China;State Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute ofBotany, Chinese Academy of Sciences, Kunming 650204,China |
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| Abstract: | The petroleum either fraction of ethanol extract of Acorus tatarinowii were separated by column chromatography and recrystallization to afford seven compounds.On the spectroscopic analysis,they were identified as 1-hydroxy-7(11),9-guaiadien-8-one( 1 ), calamenone( 2 ), cis-asarone( 3 ), chrysophanol( 4 ), physcion( 5 ), emodin( 6 ), (+)-galbacin( 7 ). Compound 1 is a new compound. Compounds 4-7 were isolated from this plant for the first time. |
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| Keywords: | Acorus tatarinowii sesquiterpene chemical compounds |
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