| 三春水柏枝化学成分的研究Ⅰ |
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| 引用本文： | 李帅,陈若芸,于德泉.三春水柏枝化学成分的研究Ⅰ[J].中国中药杂志,2007,32(5):403-406. |
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| 作者姓名： | 李帅 陈若芸 于德泉 |
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| 作者单位： | 中国医学科学院,中国协和医科大学,药物研究所,北京,100050 |
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| 摘 要： | 目的：研究三春水柏枝的化学成分。方法：用硅胶柱色谱法分离,用理化性质及波谱方法鉴定结构。结果：从石油醚部位分离鉴定了4个化合物：3-羰基-14-taraxeren-28-醛(1),3-羰基-14-taraxeren-28-醇(2),表无羁萜醇(3),4-甲基-豆甾-7-烯-3-醇(4)；从醋酸乙酯部位分离鉴定了3个化合物：morelloflavone(5),3,5-二羟基-4-甲氧基-苯甲酸甲酯(6),3-羟基-4-甲氧基-反式桂皮酸(7)。结论：以上均为首次从该属植物中分离得到。
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| 关 键 词： | 水柏枝 化学成分 三萜 甾醇 酚酸 |
| 文章编号： | 1001-5302（2007）05-0403-04 |
| 收稿时间： | 2006-06-19 |
| 修稿时间： | 2006-06-19 |
Study on chemical constituents of Myricaria paniculata Ⅰ |
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| LI Shuai; CHEN Ruo-yun; YU De-quan.Study on chemical constituents of Myricaria paniculata Ⅰ[J].China Journal of Chinese Materia Medica,2007,32(5):403-406. |
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| Authors: | LI Shuai; CHEN Ruo-yun; YU De-quan |
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| Institution: | Institute of Materia Medica , Chinese Academy of Medical Sciences, Peking Union Medical College, Beijing 100050, China |
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| Abstract: | Objective: To study the chemical constituents of Myricaria paniculata. Method: Silica gel column chromatography was used to separate and purify the chemical constituents, and the structures were elucidated by spectral analysis. Result: Four compounds were isolated from the petroleum ether soluble portion, identified as 28-aldehyde-taraxerenone (1), 28-hydroxy-taraxerenone (2), epi-friedelanol (3), 4-methyl stigmast-7-en-3-ol (4). Three compounds were isolated from the EtOAc soluble portion, identified as morelloflavone (5), methyl 3, 5-dihydroxy-4-methoxybenzoate (6), 3-hydroxy-4-methoxy cinnamic acid (7). Conclusion: All of these compounds were isolated from the genus for the first time. |
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| Keywords: | Myricaria paniculata chemical constituents triterpenoid sterol phenol acid |
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