| 银杏叶提取物及制剂萜类内酯薄层色谱荧光扫描定量测定研究 |
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| 引用本文： | 颜玉贞,谢培山,钱浩良,林巧玲. 银杏叶提取物及制剂萜类内酯薄层色谱荧光扫描定量测定研究[J]. 中国中药杂志, 1997, 22(3): 159-162 |
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| 作者姓名： | 颜玉贞 谢培山 钱浩良 林巧玲 |
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| 作者单位： | 广州市药品检验所 广州 510160 |
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| 摘 要： | 建立了采用优化条件展开的薄层色谱进行热化学衍生荧光,原位薄层定量,同板同时测定银杏内酯A,B,C及白果内酯,最低检出限分别为0.12～0.35μg。灵敏度分别为0.25～0.5μg,较HPLC示差折光检测器提高约10倍,分析时效比提高6倍以上,精密度同板RSD2%～3%,异板RSD2.3%～3.7%,回收率95.3%～98.8%。
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| 关 键 词： | 银杏叶 萜类内酯 原位荧光薄层色谱测定 |
| 收稿时间： | 1996-11-06 |
Study on Assay of Terpenes in the Leaves of Ginkgo biloba Extract and Its Preparations by insitu Fluorometric TLC |
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| Yan Yuzhen;Xie Peishan;Qian Haoquan; Lin Qiaoling. Study on Assay of Terpenes in the Leaves of Ginkgo biloba Extract and Its Preparations by insitu Fluorometric TLC[J]. China Journal of Chinese Materia Medica, 1997, 22(3): 159-162 |
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| Authors: | Yan Yuzhen Xie Peishan Qian Haoquan Lin Qiaoling |
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| Abstract: | A new TLC method for the assay of terpene lactones in Ginkgo biloba extract and its preparations has been established by means of optimized development condition and post chromatographic thermal fluorescence derivatization. Satisfactory results can be obtained through polynomial regression calibration. The data obtained by this method have been proved ten times higher in sensitivity than those obtained by HPLC refracto detector. |
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| Keywords: | Ginkgo biloba terpene lactone fluorometric TLC |
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