| 小叶黑柴胡药材的HPLC指纹图谱研究 |
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| 引用本文： | 刘鄂湖,蔡光明,朱海升,黄鹤慧,周伟,熊晗辉.小叶黑柴胡药材的HPLC指纹图谱研究[J].中草药,2008,39(10):1560-1562. |
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| 作者姓名： | 刘鄂湖 蔡光明 朱海升 黄鹤慧 周伟 熊晗辉 |
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| 作者单位： | 1. 解放军302医院全军中药研究所,北京,100039;湖南中医药大学药学院,湖南,长沙,410004
2. 解放军302医院全军中药研究所,北京,100039 |
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| 摘 要： | 目的建立小叶黑柴胡药材的HPLC指纹图谱。方法以Kromasil C18为色谱柱,流动相为乙腈-水梯度洗脱,体积流量1.0 mL/min,检测波长260 nm。结果建立了小叶黑柴胡药材的HPLC指纹图谱,确定了14个共有峰,共有峰相对保留时间的RSD为0.02%~1.49%,相对峰面积的RSD为6.12%~58.75%,10批样品的相似度均大于0.9。结论本方法简单可靠,可用于小叶黑柴胡药材的质量控制。
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| 关 键 词： | 小叶黑柴胡 高效液相色谱法 指纹图谱 相似度评价 |
| 收稿时间： | 1/2/2008 12:00:00 AM |
HPLC Fingerprint of Bupleurum smithii var.Parvifolia |
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| LIU E-hu,CAI Guang-ming,ZHU Hai-sheng,HUANG He-hui,ZHOU Wei and XIONG Han-hui.HPLC Fingerprint of Bupleurum smithii var.Parvifolia[J].Chinese Traditional and Herbal Drugs,2008,39(10):1560-1562. |
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| Authors: | LIU E-hu CAI Guang-ming ZHU Hai-sheng HUANG He-hui ZHOU Wei and XIONG Han-hui |
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| Institution: | 302 Hospital of PLA & PLA Institute of Chinese Materia Medica, Beijing 100039, China;School of Pharmacy, Hunan University of Tradilional Chinese Medicine, Changsha 410004, China;302 Hospital of PLA & PLA Institute of Chinese Materia Medica, Beijing 100039, China;302 Hospital of PLA & PLA Institute of Chinese Materia Medica, Beijing 100039, China;302 Hospital of PLA & PLA Institute of Chinese Materia Medica, Beijing 100039, China;302 Hospital of PLA & PLA Institute of Chinese Materia Medica, Beijing 100039, China;School of Pharmacy, Hunan University of Tradilional Chinese Medicine, Changsha 410004, China;302 Hospital of PLA & PLA Institute of Chinese Materia Medica, Beijing 100039, China;School of Pharmacy, Hunan University of Tradilional Chinese Medicine, Changsha 410004, China |
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| Abstract: | |
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| Keywords: | Bupleurum smithii Wolff var parvifolia Shan et Y Li HPLC fingerprint similarity evaluation |
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