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丹参中丹参酮ⅡA受热含量降低的规律研究
引用本文:杜志谦,冯坤,刘月桂,赵新杰,王广强,薛素娟.丹参中丹参酮ⅡA受热含量降低的规律研究[J].中草药,2002,33(10):892-893.
作者姓名:杜志谦  冯坤  刘月桂  赵新杰  王广强  薛素娟
作者单位:河南省洛阳正骨研究所、正骨医院,河南,洛阳,471002
摘    要:目的研究丹参药材中的丹参酮ⅡA受热含量降低的变化规律.方法采用化学动力学法,并采用HPLC法测定丹参在70℃,80℃,90 ℃,100 ℃四个温度加热不同时间丹参酮ⅡA含量.结果丹参酮ⅡA的含量(lgC)与加热时间(t)呈直线关系,K7.℃=2.378 9×10-3h-1,K80℃=7.217 6×10-3h-1,K90℃=2.060 49×10-2h-1,K100℃=5.628 5×10-2h-1.结论丹参酮ⅡA的分解属一级反应,lgK=14.386 4-5 834.316 7/T,t25℃0.9=1.9年.

关 键 词:丹参  丹参酮ⅡA  化学动力学  HPLC  高效液相色谱法  含量测定
文章编号:0253-2670(2002)10-0892-02
收稿时间:2002/1/25 0:00:00
修稿时间:2002年1月25日

Regularity of lowering heated contents of tanshinone ⅡA in root of Salvia miltiorrhiza
DU Zhi qian,FENG Kun,LIU Yue gui,ZHAO Xin jie,WANG Guang qiang and XUE Su juan.Regularity of lowering heated contents of tanshinone ⅡA in root of Salvia miltiorrhiza[J].Chinese Traditional and Herbal Drugs,2002,33(10):892-893.
Authors:DU Zhi qian  FENG Kun  LIU Yue gui  ZHAO Xin jie  WANG Guang qiang and XUE Su juan
Institution:Luoyang Institute of Traditional Chinese Orthopedics and Traumatology of Henan Province, Luoyang 471002, China;Luoyang Institute of Traditional Chinese Orthopedics and Traumatology of Henan Province, Luoyang 471002, China;Luoyang Institute of Traditional Chinese Orthopedics and Traumatology of Henan Province, Luoyang 471002, China;Luoyang Institute of Traditional Chinese Orthopedics and Traumatology of Henan Province, Luoyang 471002, China;Luoyang Institute of Traditional Chinese Orthopedics and Traumatology of Henan Province, Luoyang 471002, China;Luoyang Institute of Traditional Chinese Orthopedics and Traumatology of Henan Province, Luoyang 471002, China
Abstract:
Keywords:HPLC
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