| HPLC法测定其查日嘎那-11中的甘草苷的含量 |
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| 引用本文： | 石妍,;格根塔娜,;成志平.HPLC法测定其查日嘎那-11中的甘草苷的含量[J].疾病监测与控制杂志,2009(4):209-210. |
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| 作者姓名： | 石妍 ;格根塔娜 ;成志平 |
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| 作者单位： | [1]包头市第四医院,内蒙古包头014030; [2]包头市药品检验所,内蒙古包头014030 |
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| 摘 要： | 目的建立其查日嘎那-11（甘草，沙棘，玉竹，北沙参，甘松和香附等组成）中的甘草苷的含量。方法采用HPLC测定制剂中甘草苷含量。结果HPLC测定甘草苷在0．1953-0．5207ug范围内呈良好的线性关系（r=0．99993）。平均回收率为98．82％，RSD=0．23％。结论方法简便可行，重现性好，结果准确。可有效地控制其查日嘎那-11的含量。
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| 关 键 词： | 其查日嘎那-11 甘草苷 HPLC |
Assay Of Liquiritin In Qicharigana-11 By Hplc Yang Shuping Gegen Tana Cheng Zhiping |
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| Institution: | SHI yan, Gegentana, CHENG Zhi-Ping(1.The Forth Hospital ofBaotou, Baotou 014030; 2.Baotou Institute for Durg Control, Baotou 014030, China) |
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| Abstract: | Objective To establish methods of quality control of QichaRigana- 11 （Radix et Rhizoma Glycyrrhizae,Fructus Hippophae,Rhizoma Polygonati Odorati,Radix Glehniae,Radix et Rhizoma Nardostachyos,Rhizoma Cyperi,etc.） Methods Radix et Rhizoma Glycyrrhizae and Radix Aucklandiae was identified by TLC and the ingredients of Liquiritin were determined by HPLC.Resuits The spots of TLC is clear .The linear range of liquirifin was from 0.1953-0.5207ug （r=0.99993） .The average recovery was 98.82% and RSD=0.23%,respectively.Conelusion This method is proved to be fast ,simple and accurate. It can be used effectively for quality control of the preparation. |
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| Keywords: | QichaRigana-11 quality standard HPLC |
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