| 高速分散液相色谱法测定毒饵中的溴敌隆 |
| |
| 引用本文： | 方赤光,方群欣.高速分散液相色谱法测定毒饵中的溴敌隆[J].中国媒介生物学及控制杂志,1995,6(3):193-194. |
| |
| 作者姓名： | 方赤光 方群欣 |
| |
| 作者单位： | 吉林省卫生防疫站，东北师范大学化学系 |
| |
| 摘 要： | 本文介绍了高效液相色谱法测定毒饵中的溴敌隆，样品经高速分散器萃取后直接进行分析，紫外检测器波长设定２８０ｎｍ，色谱柱为ＹＷＧ－Ｃ１８Ｈ３７，分析结果的相对标准偏差为１．８％，回收率为９２．４％，可简便、快速测定含量在０．００５％左右的溴敌隆毒饵，亦可有效地分离鉴定杀鼠迷和杀鼠灵等香豆素类杀鼠剂。
|
| 关 键 词： | 溴敌隆 灭鼠药 毒饵 药物鉴定 液相色谱 |
High Speed Despersive Determination of Bromadiolone in Rodent Baits by Liquid Chromatography |
| |
| Pang Chi-guang, Li Qing, Fang Qun-xin et al..High Speed Despersive Determination of Bromadiolone in Rodent Baits by Liquid Chromatography[J].Chinese Journal of Vector Biology and Control,1995,6(3):193-194. |
| |
| Authors: | Pang Chi-guang Li Qing Fang Qun-xin |
| |
| Abstract: | A method was described for the determination of bromadiolone in rodent baits.Samples were extracted with high speed despersion,then they were determinated by liguid chromatography with UV detection at 280nm.Chromatography was performed with a YWG- C18H37 column. The method was tested for precision,linearlty and recovery.Analyses of ten samples gave a mean relative standard deviation of 4.6%.Linearity was 0.997.Recovery from samples was 92.4%. The method could be applicable to rodent formulations with bromadiolone content 0.005%. |
| |
| Keywords: | Brmadiolone High speed despersion Liguid chromatography |
| 本文献已被 CNKI 维普 等数据库收录！ |
