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| 香加皮抗心力衰竭有效部位的制备工艺研究* | |
| 引用本文： | 杨虹,刘虹,任晓亮,王萌,朱晓月. 香加皮抗心力衰竭有效部位的制备工艺研究*[J]. 天津中医药大学学报, 2011, 30(3): 169-171 |
| 作者姓名： | 杨虹 刘虹 任晓亮 王萌 朱晓月 |
| 作者单位： | 1. 300193,天津中医药大学 2. 教育部方剂学重点实验室, 天津中医药大学中医药研究院,300193 |
| 基金项目： | 围家科技支撑计划“重大新药创制”重大专项 |
| 摘 要： | [目的]对香加皮抗心力衰竭有效部位的制备工艺进行研究。[方法]采用制备性快速柱结合精制柱的分步富集法制备香加皮有效部位,分别考察了制备性快速柱的洗脱溶剂、硅胶用量和精制柱的径高比。[结果]确定的制备工艺使有效部位中杠柳毒苷的含量达到50%以上。[结论]确定的香加皮抗心力衰竭有效部位制备工艺稳定、经济、重复性好。 |
| 关 键 词： | 香加皮 有效部位 杠柳毒苷 |
Study on preparation technology of effective fraction for anti-heart failure in Cortex Periplocae(Xiangjiapi) |
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| YANG Hong,LIU Hong,REN Xiao-liang,WANG Men and ZHU Xiao-yue. Study on preparation technology of effective fraction for anti-heart failure in Cortex Periplocae(Xiangjiapi)[J]. Journal of Tianjin University of Traditonal Chinese Medicine, 2011, 30(3): 169-171 | |
| Authors: | YANG Hong LIU Hong REN Xiao-liang WANG Men ZHU Xiao-yue |
| Affiliation: | YANG Hong1,LIU Hong2,REN Xiao-liang2,et al (1.Tianjin University of TCM,Tianjin 300193,China; 2.Research Institute of Tianjin University of TCM;Key Laboratory of Pharmacology of TCM Formulae, Ministry of Education,Tianjin 300193,China) |
| Abstract: | [Objective] To study the preparation technology of effective fraction for anti-heart failure in Cortex Periplocae(Xiangjiapi).[Methods] The effective fraction was prepared by the combination of fast-preparation column and refining column.The ratio of raw material to silica gel and ratio of diameter to height were investigated.[Results] By the determined technology,the contents of periplocin in effective fractions were above 50%.[Conclusion] The preparation technology of the effective fraction for anti-heart failure in Cortex Periplocae is stable,economic and reproducible. |
| Keywords: | Cortex Periplocae effective fraction periplocin |
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