| HPLC法测定血元通颗粒中二苯乙烯苷的含量 |
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| 引用本文： | 顾燕飞,朱法根,沈治平,赵文艳.HPLC法测定血元通颗粒中二苯乙烯苷的含量[J].海峡药学,2014,0(7):67-69. |
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| 作者姓名： | 顾燕飞 朱法根 沈治平 赵文艳 |
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| 作者单位： | 顾燕飞(济川药业集团有限公司泰兴225441)；朱法根(济川药业集团有限公司泰兴225441)；沈治平(济川药业集团有限公司泰兴225441)；赵文艳(济川药业集团有限公司泰兴225441)； |
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| 摘 要： | 目的建立HPLC法测定血元通颗粒中二苯乙烯苷含量的方法。方法以十八烷基硅烷键合硅胶为填充剂，流动相为乙腈：水（18：82），检测波长为320nm，流速1．0mL·min^-1，柱温30℃。结果二苯乙烯苷浓度在5．80～87．06μg·mL^-1范围内呈良好的线性关系，r=0．9998。加样回收率为99．9％，RSD为1．54％。结论该方法操作简便、灵敏、可靠，可用于血元通颗粒的质量控制。
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| 关 键 词： | 二苯乙烯苷 血元通颗粒 高效液相色谱法 |
Determination of Stilbeneglucoside in Xueyuantong Granules by HPLC |
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| GU Yan-fei,ZHU Fa-gen,SHEN Zhi-ping,ZHAO Wen-yan.Determination of Stilbeneglucoside in Xueyuantong Granules by HPLC[J].Strait Pharmaceutical Journal,2014,0(7):67-69. |
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| Authors: | GU Yan-fei ZHU Fa-gen SHEN Zhi-ping ZHAO Wen-yan |
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| Institution: | (Jiangsu Jumpcan Pharmaceutical Group Co., Ltd. ,Taixing 225441, China) |
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| Abstract: | OBJECTIVE To establish a HPLC method for the determination of stilbeneglucoside in Xueyuantong Granules. METHODS Octadecylsilane chemically bonded silica was used as bulking agent. The mobile phase was consisted of acetonitrile-water （18：82） with the flow rate of 1.0mL · min^-1, and the detection wavelength was 320nm,with the column temperature at 30℃. RESULTS Stilbeneglucoside showed a good linearity in the concentraterange of 5.80 - 87.06μg · mL^-1 , the coefficent was 0. 9998, and the average recovery was 99.9% （ RSD = 1.54% ）. CONCLUSION The method is simple,sensitive and suitable,can be used for the＇quality control of Xueyuantong Granules. |
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| Keywords: | Stilbeneglucoside Xueyuantong Granules HPLC |
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