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| 升血颗粒质量标准研究 | |
| 引用本文： | 戴晓雁,王玉洁,魏学兵. 升血颗粒质量标准研究[J]. 西部中医药, 2014, 0(1): 31-34 |
| 作者姓名： | 戴晓雁 王玉洁 魏学兵 |
| 作者单位： | 戴晓雁 (甘肃省肿瘤医院,甘肃 兰州,730050)； 王玉洁 (甘肃省肿瘤医院,甘肃 兰州,730050)； 魏学兵 (甘肃省药品检验所)； |
| 摘 要： | 目的：建立升血颗粒的质量标准。方法：采用薄层色谱（TLC）法对升血颗粒中山茱萸、黄芪、丹参、麦门冬进行定性鉴别；采用高效液相色谱法对升血颗粒中马钱苷的含量进行定量测定。结果：TLC 斑点清晰、分离度好，阴性对照无干扰；马钱苷进样量在0.0752～0.451μg/mL范围内与峰面积呈良好线性关系（r＝0.9983），平均加样回收率为96.2％，RSD＝2.3％（n＝6）。结论：所建立的标准可用于升血颗粒的质量控制。 |
| 关 键 词： | 升血颗粒 质量标准 薄层色谱法 高效液相色谱法 |
Study on Quality Standard of ShengXue Granules |
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| DAI Xiaoyan,WANG Yujie,WEI Xuebing. Study on Quality Standard of ShengXue Granules[J]. Western Journal of Traditional Chinese Medicine, 2014, 0(1): 31-34 | |
| Authors: | DAI Xiaoyan WANG Yujie WEI Xuebing |
| Affiliation: | DAI Xiaoyan, WANG Yujie, WEI Xuebing |
| Abstract: | Objective：To establish quality control of ShengXue granules. Methods：ShanZhuYu（Cornus offici-nalis）, HuangQi （radix Astragalus）, DanShen （radix salviae miltiorrhizae） and MaiMenDong [Ophitopogin japonicum （L.f） Ker.-Gawl.] in ShengXue granules were identified by TLC;the contents of loganin were determined by HPLC. Results：TCL figures were distinct and reproducible, the blank test showed no interference;loganin showed better linear relationship in the range between 0.0752 and 0.451μg/mL and peak areas （r=0.998 3）, average recovery rate was 96.2%, RSD=2.3%（n=6）. Conclusion：The standard could be used in quality control of ShengXue granules. |
| Keywords: | ShengXue granules quality control TLC HPLC |
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