| 狼毒大戟的化学成分研究 |
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| 引用本文： | 孙增玉,张秋梅.狼毒大戟的化学成分研究[J].辽宁中医杂志,2014(1):141-143. |
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| 作者姓名： | 孙增玉 张秋梅 |
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| 作者单位： | 辽宁中医药大学附属医院,辽宁沈阳110032 |
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| 摘 要： | 目的:研究狼毒大戟根的化学成分。方法:利用反复硅胶柱和凝胶柱层析进行分离和纯化,通过理化性质和波谱数据鉴定化合物结构。结果:分离得到7个化合物,分别鉴定为:23(Z)-环阿尔廷-23-稀-3β,25-二醇(1)、22(E)-环阿尔廷-22-稀-3β,25-二醇(2)、Jolkinolide B(3)、2,4-二羟基-6-甲氧基-3-醛基苯乙酮(4)、β-香树脂醇乙酸酯(5)、Antiquorin(6)、二十四亚甲基环阿尔廷醇(7)。结论:化合物7为首次从绿玉树中分离得到。
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| 关 键 词： | 狼毒大戟 化学成分 分离 鉴定 |
Chemical Constituents from Euphorbia fischeriana Steud |
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| SUN Zengyu,ZHANG Qiumei.Chemical Constituents from Euphorbia fischeriana Steud[J].Liaoning Journal of Traditional Chinese Medicine,2014(1):141-143. |
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| Authors: | SUN Zengyu ZHANG Qiumei |
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| Institution: | (Affiliated Hospital of Liaoning University of Traditional Chinese Medicine, Shenyang 110032 ,Liaoning, China) |
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| Abstract: | Objective：To study the chemical constituents of Euphorbia fischeriana Steud. Methods：The chemical constituents were isolated by repeated silica gel and Sephadex LH -20 column chromatography, and their structures were elucidated by physi- cal and spectral analyses. Results：Seven compounds were isolated and identified as 23 （Z） -cycloart -23 -en -313,25 -diol （ 1 ）, 22 （E） - cycloart - 22 - en - 313,25 - diol （ 2 ）, Jolkinolide B （ 3 ）, 2,4 - dihydroxy - 6 - methoxy - 3 - formyl - 1 - aceto- phenone （4）, 13 - Amyrin acetate （5）, Antiquorin （6）, 24 - methylenecycoartanol （ 7 ）. Conclusion ： Compound 7 was isolated from the title plant for the first time. |
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| Keywords: | Euphorbia fischeriana Steud chemical constituents isolation identification |
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