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| HPLC法测定蒙药阿那日五味散中胡椒碱的含量 | |
| 引用本文： | 巴根那,吴香杰,包桂花,白鲜子. HPLC法测定蒙药阿那日五味散中胡椒碱的含量[J]. 辽宁中医杂志, 2008, 35(1): 111-112 |
| 作者姓名： | 巴根那 吴香杰 包桂花 白鲜子 |
| 作者单位： | 内蒙古民族大学蒙医药学院,内蒙古,通辽,028000;内蒙古民族大学2007届药物制剂专业,内蒙古,通辽,028000 |
| 摘 要： | 目的:建立蒙药阿那日五味散中胡椒碱的高效液相含量测定方法。方法:使用C18色谱柱(150mm×40mm),甲醇—水(77∶23)为流动相,流速为:0.6mL/min,检测波长:343nm。结果:胡椒碱的线性范围为0.0285~0.1425μg,(r=0.9999)。平均回收率为98.33%,RSD=0.98%。结论:该实验方法简便易行,结果准确可靠,可用于蒙药阿那日五味散质量控制指标。 |
| 关 键 词： | 高效液相色谱法 蒙药阿那日五味散 胡椒碱 含量 |
| 文章编号： | 1000-1719（2008）01-0111-02 |
| 收稿时间： | 2007-08-27 |
| 修稿时间： | 2007-08-27 |
Determination of Piperine in Mongolian Medicine Anariwuweisan the Content of HPLC |
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| BA Gen-na,WU Xiang-jie,BAO Gui-hua,BAI Xian-zi. Determination of Piperine in Mongolian Medicine Anariwuweisan the Content of HPLC[J]. Liaoning Journal of Traditional Chinese Medicine, 2008, 35(1): 111-112 | |
| Authors: | BA Gen-na WU Xiang-jie BAO Gui-hua BAI Xian-zi |
| Abstract: | Objective:Finding the methods of determining the high efficiency liquid phase content of pepper alkali in Mongolian medicine Anariwuweisan FSA Powder.Methods:Using,C18 color spectrum column,methanol-water(77∶23) being mobile phase;Velocity of flowing:0.6mL/min;Examining wavelength: 343nm.Result:Linear range of pepper alkali is 0.0285～0.1425μg,and the average recovery rate is 98.33%,RSD=0.98%.Conclusion:The ways of the experiment is easy to operate,and the result is reliable.It can be used as the quality controlling indicator of Mongolian medicine Anariwuweisan FSA Powder. |
| Keywords: | HPLC Mongolian medicine Anariwuweisan FSA Powder pepper alkali content |
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