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| 动物类生药的鉴别研究——6.全蝎的鉴别 | |
| 引用本文： | 李振荣,聂凤禔,张春宝. 动物类生药的鉴别研究——6.全蝎的鉴别[J]. 河北医科大学学报, 1987, 0(3) |
| 作者姓名： | 李振荣 聂凤禔 张春宝 |
| 作者单位： | 河北医学院生药学教研室,河北医学院生药学教研室,河北医学院药学系 80级学生 |
| 摘 要： | 全蝎粉末显微特征主要为两种刚毛及体壁碎片,体壁碎片上有多边形纹理、圆形乳头状突起及毛窝。纸层析用正丁醇—冰醋酸—乙醇—水(4:1:1:2)做展开剂,0.5％茚三酮显色,显3个斑点,只Rf值为0.26、0.34、0.45。纸上电泳爪甲酸—乙酸缓冲液,200V恒压电泳2.5小时,0.5％茚三酮显色,显7个斑点,泳动值为6.4、11.3、12.4、14.1、15.2、17.1、17.9(cm)。紫外光谱测定在258.9nm处显示最大吸收。 |
| 关 键 词： | 全蝎 解剖学与组织学 色谱法 纸层 电泳 纸层 分光光度测定法 紫外线 |
PHARMACOGNOSTICAL STUDY ON THE CHINESE CRUDE DRUG "QUAN XIE" (SCORPION) |
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| Li Zhenrong Nie Fengzhe Zhang Chunbao. PHARMACOGNOSTICAL STUDY ON THE CHINESE CRUDE DRUG "QUAN XIE" (SCORPION)[J]. Journal of Hebei Medical University, 1987, 0(3) | |
| Authors: | Li Zhenrong Nie Fengzhe Zhang Chunbao |
| Affiliation: | Li Zhenrong Nie Fengzhe Zhang Chunbao Department of Pgarmacognacy |
| Abstract: | Two different bristles and fragments of body wall were the powder features on the chinese crude drug "QUAN XIE" There are polygonal grains, papillaes and hair cavits on the surface of the fragments of body wall. Three spots Rf value at 0.26, 0.34, 0.45 were showed by paper-layer chromatography with n-butyl alcohol; ice acetic acid; ethyl alcohol; water(4:1=1:2). After paper electrophoresis with buffer salution of formic-acetic acid and apraying 0.5% Ninhydrin solution, it shows R.M.at 6.4, 11.3, 12.4, 14.1, 15.2, 17.1, 17.9, (cm).An absorption peak at 258.gnm was determined by UV absorption spectrum. |
| Keywords: | QUAN XIE(scorpion) anatomy and histology paper chromatography electrophoresis ultraviolet spectrophotometry |
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