| 赶山鞭的化学成分分析Ⅱ |
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| 引用本文： | 董建勇,贾忠建. 赶山鞭的化学成分分析Ⅱ[J]. 中国中药杂志, 2005, 30(20): 1595-1597 |
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| 作者姓名： | 董建勇 贾忠建 |
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| 作者单位： | 1. 温州医学院,药学院,浙江,温州,325035;兰州大学,功能有机化学国家重点实验室,甘肃,兰州,730000
2. 兰州大学,功能有机化学国家重点实验室,甘肃,兰州,730000 |
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| 摘 要： | 目的:对赶山鞭的化学成分进行分析。方法:用色谱技术分离,根据理化性质和IR,NMR,MS等光谱技术鉴定化合物结构。结果:分离并鉴定出9个化合物。分别为4-羟基苯甲酸(1),6,9-dihydroxy-4,7-megastigmadien-3-one(2),丁醇-O-α-D-果糖苷(3),24-ethyl-cholest-7-ene-3β,5α,6-βtriol(4),已醇(5),1β,6α-二羟基桉烷-4(14)-烯(6),β-谷甾醇(7),5,5-二甲基-4-羟基-四氢呋喃-2-酮(8),β-胡萝卜苷(9)。结论:均为首次从该植物中分到。
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| 关 键 词： | 赶山鞭 化学成分 |
| 文章编号： | 1001-5302（2005）20-1595-03 |
| 收稿时间： | 2004-10-15 |
| 修稿时间： | 2004-10-15 |
Study on the chemical constituents in herb of Hypericum attenuatum |
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| DONG Jian-yong;JIA Zhong-jian. Study on the chemical constituents in herb of Hypericum attenuatum[J]. China Journal of Chinese Materia Medica, 2005, 30(20): 1595-1597 |
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| Authors: | DONG Jian-yong JIA Zhong-jian |
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| Affiliation: | 1. Department of Pharmacology, Wenzhou Medical College, Wenzhou 325035, China ; 2. National laboratory of Applied Organic Chemistry, Lanzhou University, Lanzhou 730000, China |
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| Abstract: | OBJECTIVE: To study the constituents of Hypericum attenatum. METHOD: The compounds were isolated by chromatography on silica gel, the structures were identified by their physical, chemical properties and IR, NMR and MS spectral data respectively. RESULT: Nine compounds were isolated and identified as p-hydroxybenzoic acid (1), 6, 9-dihydroxy-4, 7-megastigmadien-3-one (2), butyl alcohol-O-alpha-D-fructoside (3), 24-ethyl-cholest-7-ene-3 beta, 5 alpha, 6 beta-thtroil (4), hexanol (5), 1 beta, 6 alpha-dihydroxyeudesmane-4(14)-ene (6), beta-sitosterol (7), 5, 5-dimethyl-4-hydroxy-tetrahydrofuran-2-one (8), beta-daucosterol (9). CONCLUSION: All of the compounds were isolated from H. attenuatum for the first time. |
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| Keywords: | Hypericum attenuatum chemical constituents |
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