| HPLC测定大血藤药材中绿原酸的含量 |
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| 引用本文： | 丁越,张永,丁文平,张彤,陶建生,荣蓉. HPLC测定大血藤药材中绿原酸的含量[J]. 中国实验方剂学杂志, 2013, 19(4): 99-102 |
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| 作者姓名： | 丁越 张永 丁文平 张彤 陶建生 荣蓉 |
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| 作者单位： | 上海中医药大学,上海,201203 |
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| 基金项目： | 上海市科委资助项目(09dZ1975500);上海市人才发展基金项目(20111015);上海市教委基金项目(10SG40,J50302) |
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| 摘 要： | ![]()
目的:建立大血藤药材中绿原酸的含量测定方法.方法:采用高效液相色谱法,Diamonsil ODS-C18色谱柱(4.6mm×250 mm,5μm),流动相乙腈-4％磷酸水(11∶89),流速1.0 mL· min-1,检测波长327 nm,柱温25℃.结果:绿原酸在0.000 102 ～0.010 2 mg线性关系良好.加样回收率为102.4％,RSD 1.7％ (n =6).结论:采用HPLC测定大血藤药材中绿原酸的含量,样品处理方法便捷,测定方法简单,结果准确可靠,可用于大血藤饮片、大血藤制剂的质量控制.
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| 关 键 词： | 绿原酸 高效液相色谱法 含量测定 大血藤 |
| 收稿时间： | 2012-01-04 |
Determination of Chlorogenic Acid in Sargentodoxa cuneata by High Performance Liquid Chromatography |
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| DING Yue,ZHANG Yong,DING Wen-ping,ZHANG Tong,TAO Jian-sheng and RONG Rong. Determination of Chlorogenic Acid in Sargentodoxa cuneata by High Performance Liquid Chromatography[J]. China Journal of Experimental Traditional Medical Formulae, 2013, 19(4): 99-102 |
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| Authors: | DING Yue ZHANG Yong DING Wen-ping ZHANG Tong TAO Jian-sheng RONG Rong |
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| Affiliation: | Shanghai University of Traditional Chinese Medicine, Shanghai 201203, China;Shanghai University of Traditional Chinese Medicine, Shanghai 201203, China;Shanghai University of Traditional Chinese Medicine, Shanghai 201203, China;Shanghai University of Traditional Chinese Medicine, Shanghai 201203, China;Shanghai University of Traditional Chinese Medicine, Shanghai 201203, China;Shanghai University of Traditional Chinese Medicine, Shanghai 201203, China |
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| Abstract: | ![]()
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| Keywords: | chlorogenic acid HPLC content determination Sargentodoxa cuneata |
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