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薄层扫描法测定香连丸中盐酸小檗碱的含量
引用本文:周华平,宋广聪,王仁英.薄层扫描法测定香连丸中盐酸小檗碱的含量[J].现代中药研究与实践,2000(5).
作者姓名:周华平  宋广聪  王仁英
作者单位:安徽省合肥神鹿药业有限公司!230041
摘    要:目的 :测定香连丸中盐酸小檗碱的含量。方法 :采用薄层扫描法和分光光度法测定盐酸小檗碱的含量。应用 t检验考察二种方法之间是否存在显著性差异。结果 :薄层扫描法可排除其它生物碱的干扰 ,平均回收率为 99.75 % ,RSD=1.5 6 % ,方法简单、准确 ,重现性好。二种方法存在显著性差异。结论 :本法可作为香连丸的含量测定

关 键 词:香连丸  分光光度法  薄层扫描法  盐酸小檗碱  含量测定

Determination of Berberine Hydrochloride in Xianglian Pills by TLC scanning
Song Guangcong,Wang Renying.Determination of Berberine Hydrochloride in Xianglian Pills by TLC scanning[J].Research and Practice on Chinese Medicines,2000(5).
Authors:Song Guangcong  Wang Renying
Abstract:OBJECTIVE:To determine the content of Berberine hydrochloride in Xianglian pills.METHOD:Using TLC scanning and spectrophotography to determinate the content of berberine hydrochloride.Examining the significant difference between the two methods with T test.RESULTS:TLC scanning can remove the interference of other alklorids,the average recovery is 99.75%,RSD=1.56%,this method is simple,accurate and with a good reproducibility.It is a significant difference between the two methods.CONCLUSION:This method can determinate the content of Xianglian pills.
Keywords:Xianglian pills  spectrophotography  TLC  scanning  Berberine hydrochloride  determination  
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