| UPLC同时测定复方守宫散中核苷类含量 |
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| 引用本文： | 吴健,高家荣,韩燕全,李翔.UPLC同时测定复方守宫散中核苷类含量[J].中国现代应用药学,2014,31(7):843-846. |
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| 作者姓名： | 吴健 高家荣 韩燕全 李翔 |
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| 作者单位： | 安徽中医药大学第一附属医院,安徽中医药大学第一附属医院,安徽中医药大学,安徽中医药大学第一附属医院,安徽中医药大学第一附属医院 |
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| 基金项目： | 国家中医药重点学科(临床中药学)建设项目(国中医药人教发[2012]32号)；安徽中医药大学青年科学研究基金项目(2013qn019) |
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| 摘 要： | 目的 建立UPLC法同时测定复方守宫散中腺嘌呤、腺苷含量的方法。方法 用Acquity BEH C18(2.1 mm×100 mm,1.7 μm),甲醇-水为流动相,梯度洗脱,流速0.25ml/min,柱温26℃,检测波长254nm。结果 腺嘌呤、腺苷的进样量分别在0.0409~0.5115μg(r=0.9999)、0.0578~0.7220μg(r=0.9996)范围内与其峰面积呈良好的线性关系；平均回收率分别为92.83%、94.90%,RSD分别为1.11%、1.70%。结论 该方法快速、可靠、准确,可作为复方守宫散的质量控制方法。
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| 关 键 词： | 超高效液相色谱 复方守宫散 腺嘌呤 腺苷 含量测定 |
| 收稿时间： | 2013/9/22 0:00:00 |
| 修稿时间： | 2014/2/10 0:00:00 |
Simultaneous Determination of Nucleoside Contents in Compound Shougong Powder by UPLC |
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| WU Jian,GAO Jiarong,HAN Yanquan and LI Xiang.Simultaneous Determination of Nucleoside Contents in Compound Shougong Powder by UPLC[J].The Chinese Journal of Modern Applied Pharmacy,2014,31(7):843-846. |
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| Authors: | WU Jian GAO Jiarong HAN Yanquan and LI Xiang |
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| Institution: | The first Affiliated Hospital of Anhui University of Chinese Medicine,Grade Laboratory of TCM Preparation,State Administration of TCM,Anhui Hefei,The first Affiliated Hospital of Anhui University of Chinese Medicine,Grade Laboratory of TCM Preparation,State Administration of TCM,Anhui Hefei,Anhui University of Chinaese Medicine,Anhui Hefei,The first Affiliated Hospital of Anhui University of Chinese Medicine,Grade Laboratory of TCM Preparation,State Administration of TCM,Anhui Hefei,The first Affiliated Hospital of Anhui University of Chinese Medicine,Grade Laboratory of TCM Preparation,State Administration of TCM,Anhui Hefei |
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| Abstract: | |
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| Keywords: | UPLC Compound Shougong powder Adenine Adenosine Content determination |
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