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| 三鼎丹胶囊中士的宁的含量测定 | |
| 引用本文： | 姬生国,王东,李娥,何方,宋飒. 三鼎丹胶囊中士的宁的含量测定[J]. 时珍国医国药, 2006, 17(1): 64-65 |
| 作者姓名： | 姬生国 王东 李娥 何方 宋飒 |
| 作者单位： | 1. 郑州大学药学院,河南,郑州,450052 2. 河南中医学院,河南,郑州,450008 3. 河南省焦作市中医医院,454100 |
| 摘 要： | 目的建立测定三鼎丹胶囊中士的宁的含量测定方法。方法以甲苯-丙酮-乙醇-浓氨溶液(16∶12∶1∶4)的上层溶液为展开剂,采用双波长反射锯齿扫描法,测定波长λS=254 nm,参比波长λR=325 nm,测定士的宁的含量。结果样品平均回收率为99.5%,板内RSD=4.48%(n=5)。结论此测定方法简单可行,重现性好,可作为该药质量控制的参考依据。 |
| 关 键 词： | 三鼎丹胶囊 士的宁 薄层扫描 |
| 文章编号： | 1008-0805(2006)01-0064-01 |
| 修稿时间： | 2005-09-07 |
Quantitative Determination of Strychnine in SanDingDan Capsule by TLC-Scanning |
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| JI Sheng-guo,WANG Dong,LI E,HE Fang,SONG Sa. Quantitative Determination of Strychnine in SanDingDan Capsule by TLC-Scanning[J]. Lishizhen Medicine and Materia Medica Research, 2006, 17(1): 64-65 | |
| Authors: | JI Sheng-guo WANG Dong LI E HE Fang SONG Sa |
| Abstract: | ObjectiveTo determine the content of Strychnine in SanDingDan Capsule.MethodsTLC was used with detecting wavelength 254 nm and reference wavelength 325 nm.ResultsThe average recovery was 99.15%,RSD(n=5) was 1.68%.ConclusionThe method is simple and feasible with good reproducibility,the results can provide a basis for establishing the quality standard of this capsule. |
| Keywords: | SanDingDan Capsule Strychnine TLC |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |