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| 2-(4-甲氧基苯基)-6-甲氧基苯并噻吩的合成 | |
| 引用本文： | 万小强,欧阳贵平,柯杨. 2-(4-甲氧基苯基)-6-甲氧基苯并噻吩的合成[J]. 遵义医学院学报, 2007, 30(1): 79-80 |
| 作者姓名： | 万小强 欧阳贵平 柯杨 |
| 作者单位： | 1. 贵州大学,精细化工研究开发中心,贵州,贵阳,550025;遵义医学院,药学系,贵州,遵义,563003 2. 贵州大学,精细化工研究开发中心,贵州,贵阳,550025 |
| 摘 要： | 目的合成目的产物2-（4-甲氧基苯基）-6-甲氧基苯并噻吩。方法以3-甲氧基苯硫酚和对甲氧基-苯乙酮为原料经溴化、烃基化、环合重排排制得目标产物。结果此法操作简便并得到高收率的标题化合物。结论改进的合成路线适合于工业化生产。 |
| 关 键 词： | 2-(4-甲氧基苯基)-6-甲氧基苯并噻吩 合成 |
| 文章编号： | 1000-2715（2007）01-0079-02 |
| 收稿时间： | 2006-12-20 |
| 修稿时间： | 2006-12-20 |
Synthesis of 2-(4-methoxypheny1)-6-methoxy-benzo[b]thiophene |
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| WAN xiao-qiang,OUYANG gui-ping,KE Yang. Synthesis of 2-(4-methoxypheny1)-6-methoxy-benzo[b]thiophene[J]. Acta Academiae Medicine Zunyi, 2007, 30(1): 79-80 | |
| Authors: | WAN xiao-qiang OUYANG gui-ping KE Yang |
| Affiliation: | Department of Pharrnic Chemistry , Zunyi Medical College , Guizhou Zunyi 563003 , China |
| Abstract: | Objective To synthesize 2-(4-methoxypheny)-6-methoxy-benzo[b]thiophene.Methods The target compound was synthesized through bromination and thioetherification from 4-methoxyacetophenone as a starting material.Results The synthetic process is simple and the yield is high.Conclusions The improved synthetic route is practical. |
| Keywords: | 2-(4-methoxypheny1)-6-methoxy-benzo[b]thiophene organic synthesis |
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