| 响应面分析法优化复方补乌糖浆微波提取工艺 |
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| 引用本文： | 陈莉,王盛,魏良兵,孟楣,冯艺戎,石金友. 响应面分析法优化复方补乌糖浆微波提取工艺[J]. 中国实验方剂学杂志, 2012, 18(2): 25-28 |
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| 作者姓名： | 陈莉 王盛 魏良兵 孟楣 冯艺戎 石金友 |
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| 作者单位： | 1. 安徽中医学院第一附属医院,合肥230031;国家中医药管理局中药制剂三级实验室,合肥 230031
2. 安徽中医学院第一附属医院,合肥,230031 |
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| 基金项目： | 安徽中医学院临床科学研究基金项目(2010LC-018A) |
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| 摘 要： | 目的:优选复方补乌糖浆的微波提取工艺参数.方法:通过响应面分析法对复方补乌糖浆微波工艺参数进行优选.结果:加水量、提取时间、微波功率对补骨脂素得率具有显著性影响,其最佳提取工艺为加药材10倍量的水,在40％微波功率下提取26 min,补骨脂素得率达到极大值,该条件下补骨脂素得率的预测值为36.33％,验证值为36.38％.结论:与原提取工艺相比,优化的微波提取工艺简便、节能、提取率高且重现性好.
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| 关 键 词： | 复方补乌糖浆 补骨脂素得率 微波提取法 响应面分析法 |
| 收稿时间： | 2011-08-31 |
Optimization of Microwave Extraction Technology Parameters for Fufang Buwu Syrup by Response Surface Analysis Method |
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| CHEN Li,WANG Sheng,WEI Liang-bing,MENG Mei,FENG Yi-rong and SHI Jin-you. Optimization of Microwave Extraction Technology Parameters for Fufang Buwu Syrup by Response Surface Analysis Method[J]. Chinese Journal of Experimental Traditional Medical Formulae, 2012, 18(2): 25-28 |
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| Authors: | CHEN Li WANG Sheng WEI Liang-bing MENG Mei FENG Yi-rong SHI Jin-you |
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| Affiliation: | First Affiliated Hospital of Anhui University of Traditional Chinese Medicine, Hefei 230031, China; State Administration of National Chinese Drugs Medicament Laboratory of Grade 3, Hefei 230031, China;First Affiliated Hospital of Anhui University of Traditional Chinese Medicine, Hefei 230031, China; State Administration of National Chinese Drugs Medicament Laboratory of Grade 3, Hefei 230031, China;First Affiliated Hospital of Anhui University of Traditional Chinese Medicine, Hefei 230031, China; State Administration of National Chinese Drugs Medicament Laboratory of Grade 3, Hefei 230031, China;First Affiliated Hospital of Anhui University of Traditional Chinese Medicine, Hefei 230031, China; State Administration of National Chinese Drugs Medicament Laboratory of Grade 3, Hefei 230031, China;First Affiliated Hospital of Anhui University of Traditional Chinese Medicine, Hefei 230031, China; State Administration of National Chinese Drugs Medicament Laboratory of Grade 3, Hefei 230031, China;First Affiliated Hospital of Anhui University of Traditional Chinese Medicine, Hefei 230031, China |
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| Abstract: | Objective:To optimize microwave extraction technology parameters of Fufang Buwu syrup.Method:Optimization of microwave extraction technology parameters for Fufang Buwu syrup by response surface analysis method.Result:Ratio of material-liquid,extraction time and microwave power had significant impact to yield of psoralen,optimum extraction conditions were as follow:ratio of material-liquid 1∶10,microwave power 40%,extraction time 26 mins.Under this technology,yield of psoralen reached maximum,with estimated value and verified value being of 36.33%,36.38%.Conclusion:This process was simple energy saving and high extraction ratio to old process,and had good reproducible. |
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| Keywords: | Fufang Buwu syrup yield of psoralen microwave extraction method response surface analysis method |
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