| 肾宝合剂质量标准研究 |
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| 引用本文： | 官启嘉,钟瑞健,周国平,谢二磊,覃玉梅,肖丽丽. 肾宝合剂质量标准研究[J]. 江西中医学院学报, 2012, 24(3): 53-57 |
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| 作者姓名： | 官启嘉 钟瑞健 周国平 谢二磊 覃玉梅 肖丽丽 |
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| 作者单位： | 江西省食品药品检验所 南昌330046 |
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| 摘 要： | 目的:建立肾宝合剂的质量控制方法.方法:采用薄层色谱法对方中所含的淫羊藿、何首乌、黄芪、补骨脂、当归、川芎进行定性鉴别；用高效液相色谱测定方中所含淫羊藿苷的含量.结果:薄层色谱法可鉴别出淫羊藿、何首乌、黄芪、补骨脂、当归川芎,且阴性对照无干扰；淫羊藿苷在0.0466-0.9700μg范围内呈良好线性关系,r=0.9999,平均回收率为99.96％,RSD =0.26％.结论:本方法操作简便、准确可靠,重现性好、可作为肾宝合剂的质量控制方法.
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| 关 键 词： | 肾宝合剂 薄层色谱法 高效液相色谱法 淫羊藿苷 质量标准 |
Study on the Quality Standard of Shenbao Heji |
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| GUAN Qi-jia , ZHONG Rui-jian , ZHOU Guo-ping , XIE Er-lei , QIN Yu-mei , XIAO Li-li. Study on the Quality Standard of Shenbao Heji[J]. Journal of Jiangxi College of Traditional Chinese Medicine, 2012, 24(3): 53-57 |
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| Authors: | GUAN Qi-jia ZHONG Rui-jian ZHOU Guo-ping XIE Er-lei QIN Yu-mei XIAO Li-li |
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| Affiliation: | Jiangxi Provincial Institute for Drug and Food Control,Nanchang330046 |
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| Abstract: | Objective: To establish the quality standard of Shenbao Heji.Methods: The six components—Epimedium brevicornum Max im,Polygonum Multiflorum,Astragalus,semen psoraleae,Angelica sinensis and Ligusticum wallichii is in Shenbao Heji were qualita tively by TLC.The contents of icariin in Shenbao Heji was determined by HPLC.Results: The TLC spots of Epimedium brevicornum Maxim,Polygonum Multiflorum,Astragalus,semen psoraleae,Angelica sinensis and Ligusticum wallichii were clear with good resolu tion and free of interference of negative samples.The linear ranges of icariin was0.0466 ～0.9700μg,the average recovery rate was 99.96%,RSD=0.26%.Conclusion: The method is rapid,accurate,sensitive and reliable,the method can be used to control the quality of Shenbao Heji. |
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| Keywords: | shenbao HeJi TLC HPLC icariin Quanlity standard |
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