| 高效液相色谱法测定银栀口服液中栀子苷的含量 |
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| 引用本文： | 李翔,刘皈阳,马建丽,周亮,高磊. 高效液相色谱法测定银栀口服液中栀子苷的含量[J]. 中国实验方剂学杂志, 2012, 18(24): 132-134 |
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| 作者姓名： | 李翔 刘皈阳 马建丽 周亮 高磊 |
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| 作者单位： | 解放军总医院第一附属医院药剂药理科,北京,100048 |
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| 摘 要： | 目的:建立测定银栀口服液中栀子苷含量的高效液相色谱方法。方法:采用Agilent Eclipse XDB-C18(4.6 mm×150 mm,5μm)色谱柱,流动相甲醇-水(25∶75),流速1.0 mL.min-1,检测波长238 nm,柱温30℃。结果:栀子苷浓度在0.010 20～0.408 0μg与峰面积线性关系良好,平均回收率为99.35%,RSD 1.90%(n=6)。结论:方法操作简便、结果准确,专属性强,可用于银栀口服液中栀子苷的含量测定。
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| 关 键 词： | 银栀口服液 栀子苷 高效液相色谱 |
| 收稿时间： | 2012-07-12 |
Determination of Geniposide in Yinzhi Oral Solution by HPLC |
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| LI Xiang,LIU Gui-yang,MA Jian-li,ZHOU Liang and GAO Lei. Determination of Geniposide in Yinzhi Oral Solution by HPLC[J]. Chinese Journal of Experimental Traditional Medical Formulae, 2012, 18(24): 132-134 |
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| Authors: | LI Xiang LIU Gui-yang MA Jian-li ZHOU Liang GAO Lei |
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| Affiliation: | Department of Pharmacy, First Affiliated Hospital of PLA General Hospital, Beijing 100048, China;Department of Pharmacy, First Affiliated Hospital of PLA General Hospital, Beijing 100048, China;Department of Pharmacy, First Affiliated Hospital of PLA General Hospital, Beijing 100048, China;Department of Pharmacy, First Affiliated Hospital of PLA General Hospital, Beijing 100048, China;Department of Pharmacy, First Affiliated Hospital of PLA General Hospital, Beijing 100048, China |
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| Abstract: | |
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| Keywords: | Yinzhi oral solution geniposide HPLC |
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